Study on Quality Control of Uyghur Medicine Preperation Yangxin Dawayi Mixike Migao

SHA La Maiti·; Ai-li; WANG Ya-li; SU Ley-man·; Ha-lik

doi:10.11653/syfj2013140108

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Study on Quality Control of Uyghur Medicine Preperation Yangxin Dawayi Mixike Migao

更新时间：2024-01-04

- Study on Quality Control of Uyghur Medicine Preperation Yangxin Dawayi Mixike Migao
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 14, Pages: 108-111(2013)
- 作者机构：
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- DOI：10.11653/syfj2013140108
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- Published：2013
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SHA La Maiti·, Ai-li, WANG Ya-li, et al. Study on Quality Control of Uyghur Medicine Preperation Yangxin Dawayi Mixike Migao[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(14): 108-111.
DOI：

SHA La Maiti·, Ai-li, WANG Ya-li, et al. Study on Quality Control of Uyghur Medicine Preperation Yangxin Dawayi Mixike Migao[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(14): 108-111. DOI： 10.11653/syfj2013140108.

摘要

目的: 建立养心达瓦依米西克蜜膏的质量标准。方法: 采用TLC法对处方中西红花、肉桂进行定性鉴别

并用RP-HPLC法测定西红花中西红花苷Ⅰ的含量;采用Luna C18(4.6 mm×250 mm

5 μm)色谱柱

甲醇-水(45:55)为流动相

流速1.0 mL·min-1

柱温35℃

检测波长440 nm

进样量10 μL。结果: 薄层鉴别专属性强

分离效果好。西红花苷Ⅰ在0.019 2~0.153 6 μg呈良好的线性关系(r=0.999 9)

平均回收率为98.7%(n=6)

RSD 1.51%。结论: 方法简便、准确、重复性好

可作为养心达瓦依米西克蜜膏的质量控制方法。

Abstract

Objective: To develop the quality standard of Yangxin Dawayi Mixike Migao. Method: The TLC method was used for the qualitative identification of Stigma Croci and Cortex Cinnamomi in the formula. The content of crocin-I in Yangxin Dawayi Mixike Migao was determined simultaneously by RP-HPLC method with a Luna C18 column (4.6 mm×250 mm

5 μm). The mobile phase was methanol-water (45:55);the flow rate was 1.0 mL·min-1. The detection wavelength was set at 440 nm

and the column temperature was set at 35℃. Result: The identification study showed strong specificity. The linear relationship was good. The linear response ranged from 6.04 μg to 45.3 μg for crocin-I and the average recovery was 98.7% with RSD 1.51%. Conclusion: The methods were simple

accurate and with a good reproducibility

and can be used for the quality control of the drug.

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Related Author

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Xia CHEN

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Related Institution

Xinjiang Uyghur Aotonomous Region Institute for Food and Drug Control

Center for Drug Evaluation，National Medical Products Administration

China Academy of Chinese Medical Sciences

Guangxi Engineering Research Center of Traditional Chinese Medicine Resource Intelligent Creation，Guangxi Key Laboratory of Medicinal Resources Protection and Genetic Improvement， Guangxi Botanical Garden of Medicinal Plants

Food and Drug Department，Ministry of Health

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