Analysis of Cleansing Mechanism of

HOU Yue-fei; DU Hong; WANG Zhe; LIU Hong-yu; LI Fei; TAN Peng; YANG Lei

doi:10.11653/syfj2013160045

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Analysis of Cleansing Mechanism of

更新时间：2024-01-04

- Analysis of Cleansing Mechanism of
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 16, Pages: 45-47(2013)
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- DOI：10.11653/syfj2013160045
  CLC：
- Published：2013
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HOU Yue-fei, DU Hong, WANG Zhe, et al. Analysis of Cleansing Mechanism of [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(16): 45-47.
DOI：

HOU Yue-fei, DU Hong, WANG Zhe, et al. Analysis of Cleansing Mechanism of [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(16): 45-47. DOI： 10.11653/syfj2013160045.

摘要

目的: 探析草乌的净制机制。方法: 采用HPLC测定3批带残茎草乌、去残茎草乌及草乌残茎中新乌头碱、乌头碱、次乌头碱、苯甲酰新乌头碱、苯甲酰乌头碱、苯甲酰次乌头碱的含量。结果: 带残茎草乌、去残茎草乌、草乌残茎中3种双酯型生物碱的总含量分别是0.59%~0.66%

0.61%~0.69%

0.39%~0.42%;3种单酯型生物碱的总含量分别是0.09%~0.10%

0.09%~0.12%

0.06%~0.08%。草乌不同部位的色谱图中除6种酯型生物碱峰外还存在共有峰4

残茎中峰4的峰面积是去残茎草乌的55%~80%。结论: 草乌残茎和去残茎草乌中6种生物碱成分含量存在差异;残茎属于生物碱成分含量较低的非药用部位

需去除。

Abstract

Objective: To analyze cleansing mechanism of Aconitum kusnezoffii. Method: HPLC was adopted to determine the content of mesaconine

aconitine

hypaconitine

benzoylmesaconine

benzoylaconitine

benzoylhypaconitine in A. kusnezoffii with stems

A. kusnezoffii without stems and stems of A. kusnezoffii. Result: The total content of three kind of diester alkaloids in A. kusnezoffii with stems

A. kusnezoffii without stems and stems of A. kusnezoffii was 0.59%-0.66%

0.61%-0.69%

0.39%-0.42%

respectively;The total content of three kind of monoester alkaloids was 0.09%-0.10%

0.09%-0.12%

0.06%-0.08%

respectively.Except six alkaloids chromatographic peaks

there was another common peak(peak 4)

area of peak 4 in stems of A. kusnezoffii was 55%-80% to that in A. kusnezoffii without stems. Conclusion: Content of six alkaloids was found in A. kusnezoffii without stems and stems of A. kusnezoffii was different.Stems of A. kusnezoffii was the non-medicinal parts whose content of six alkaloids was low

it could be removed.

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