Quality Standard for Evodiae Juice, an Adjuvant Material of Processing

HAN Xu-yang; BIAN Bao-lin; LI Rao-rao; WANG Zhi-min; YAN Li-hua; MA Yin-lian; FANG Jing

doi:10.11653/syfj2013170132

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Quality Standard for Evodiae Juice, an Adjuvant Material of Processing

更新时间：2024-01-04

- Quality Standard for Evodiae Juice, an Adjuvant Material of Processing
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 17, Pages: 132-135(2013)
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- DOI：10.11653/syfj2013170132
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- Published：2013
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HAN Xu-yang, BIAN Bao-lin, LI Rao-rao, et al. Quality Standard for Evodiae Juice, an Adjuvant Material of Processing[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(17): 132-135.
DOI：

HAN Xu-yang, BIAN Bao-lin, LI Rao-rao, et al. Quality Standard for Evodiae Juice, an Adjuvant Material of Processing[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(17): 132-135. DOI： 10.11653/syfj2013170132.

摘要

目的: 建立吴茱萸汁的质量标准。方法: 采用薄层色谱法(TLC)对吴茱萸汁进行定性鉴别

采用高效液相色谱法测定吴茱萸内酯、吴茱萸碱、吴茱萸次碱的含量

Agilent C18色谱柱(4.6 mm×250 mm

5 μm)

乙腈-水-四氢呋喃-冰醋酸(40:60:1:0.2)为流动相

流速1 mL·min-1

柱温30℃

吴茱萸内酯、吴茱萸碱检测波长为225 nm、吴茱萸次碱检测波长为343 nm。结果: 薄层鉴别专属性强

重复性良好。吴茱萸内酯

吴茱萸碱和吴茱萸次碱分别在0.12~8.10(r=0.999 9)

0.028~1.80(r=0.999 8)

0.012~0.75 μg(r=0.999 9)线性关系良好。平均回收率和RSD依次为101.49%

2.21%;102.65%

1.51%;100.47%

2.42%(n=6)。结论: 方法简便

可靠

可操作性强

适用于吴茱萸汁炮制辅料的质量控制。

Abstract

Objective: To establish the quality standard for Evodiae juice

an adjuvant material of processing. Method: The Evodiae juice was identified by TLC. The content of evodin

evodiamine and rutaecarpine in the Evodiae juice was determined by HPLC simultaneously. The column of Agilent C18 (4.6 mm×250 mm

5 μm) was used. The mobile phase consisted of acetonitrile-water-tetrahydrofuran-glacial acetic acid (40: 60: 1: 0.2). The flow rate was 1.0 mL·min-1. The wavelength was set at 225 nm for evodin and evodiamine

343 nm for rutaecarpine. Result: TLC pots were clear with strong specificity

good repeatability and easy identification. While the linear range of evodin

evodiamine and rutaecarpine were 0.12-8.10 μg (r=0.999 9)

0.028-1.80 μg (r=0.999 8)

0.012-0.75 μg (r=0.999 9). The average recoveries of three compounds were 101.49% with RSD 2.21%

102.65% with RSD 1.51% and 100.47% with RSD 3.42%(n=6) respectively. Conclusion: The method is convenient

accurate and reproducible. It can be used for the quality control of Evodiae juice

the adjuvant material.

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Related Institution

Hubei Institute for Food and Drug Control

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