Quality Standard of Ziyin Shengfa Granules

YU Ming-jie; CHEN Qing-zhu; DAI Qing; LIAO Yong; XIANG Rong-feng; CAI Yong-qing; CHEN Yong-chuan

doi:10.11653/syfj2013170143

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Quality Standard of Ziyin Shengfa Granules

更新时间：2024-01-04

- Quality Standard of Ziyin Shengfa Granules
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 17, Pages: 143-145(2013)
- 作者机构：
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- DOI：10.11653/syfj2013170143
  CLC：
- Published：2013
- 稿件说明：
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YU Ming-jie, CHEN Qing-zhu, DAI Qing, et al. Quality Standard of Ziyin Shengfa Granules[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(17): 143-145.
DOI：

YU Ming-jie, CHEN Qing-zhu, DAI Qing, et al. Quality Standard of Ziyin Shengfa Granules[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(17): 143-145. DOI： 10.11653/syfj2013170143.

摘要

目的: 建立滋阴生发颗粒的质量标准。方法: 采用薄层色谱(TLC)法对方中制何首乌、枸杞子、丹参进行定性鉴别

采用反相高效液相色谱(RP-HPLC)对方中二苯乙烯苷进行含量测定。结果: 在TLC中能检出制何首乌、枸杞子、丹参的特征斑点

阴性样品无干扰。二苯乙烯苷在0.190 5~1.143 2 μg与峰面积积分呈良好线性关系(r=0.999 9);平均加样回收率为98.60%

RSD 2.28%(n=9)。结论: 方法简单、快速、精密度高、重复性好

所建标准可用于滋阴生发颗粒质量控制。

Abstract

Objective: To establish the quality standard for Ziyinshengfa Granules. Method: The thin-layer chromatograph (TLC) method was used to identify Radix Polygoni Multiflori Preparata

Fructus Lycii

Radix Salviae Miltiorrhizae and the content of 2

5'-tetahyd roxy stilbence-2-O-β-D-glucoside was determined by RP-HPLC. Result: The characteristic spots of Radix Polygoni Multiflori Preparata

Fructus Lycii

Radix Salviae Miltiorrhizae appeared in the TLC

and there was no interference for the negative sample. The linear range of 2

5'-tetahyd roxy stilbence-2-O-β-D-glucoside was 0.190 5-1.143 2 mg·L-1 (r=0.999 9). The average recovery rates were 98.60% (RSD 2.28%) (n=9). Conclusion: This method is simple

rapid

precise and reproducible

thus it can be used for the quality control of Ziyinshengfa Granules.

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Related Author

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CHENG Yao-tang

Related Institution

Hubei Institute for Food and Drug Control

Gansu Province Hospital of Traditional Chinese Medicine

Acupuncture and Moxibustion Hospital Affiliated to Anhui College of Traditional Chinese Medicine & Anhui Modern Engineering Technology Research Center of Chinese Medicine

Jiangxi University of Chinese Medicine

Jiangxi Institute of Quality and Standardization

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