Purification of Flavonoids from  by Macroporous Resin

HE Rui-rui; ZHAN Xue-yan; TAN Peng; LIN Hong-ying; CHEN Xin; ZHAO Bao-sheng

doi:10.11653/syfj2013190093

您当前的位置：

首页 >

文章列表页 >

Purification of Flavonoids from by Macroporous Resin

更新时间：2024-01-04

- Purification of Flavonoids from by Macroporous Resin
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 19, Pages: 93-95(2013)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.11653/syfj2013190093
  CLC：
- Published：2013
- 稿件说明：
移动端阅览
HE Rui-rui, ZHAN Xue-yan, TAN Peng, et al. Purification of Flavonoids from by Macroporous Resin[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(19): 93-95.
DOI：

HE Rui-rui, ZHAN Xue-yan, TAN Peng, et al. Purification of Flavonoids from by Macroporous Resin[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(19): 93-95. DOI： 10.11653/syfj2013190093.

摘要

目的: 研究大孔树脂吸附纯化天山堇菜总黄酮的条件及参数

为黄酮类化合物的富集提供参考。方法: 比较了3种大孔树脂对天山堇菜总黄酮的吸附性能; 以天山堇菜总黄酮的得率和纯度为考察指标

对大孔树脂吸附纯化天山堇菜总黄酮的工艺进行筛选。结果: AB-8大孔树脂对天山堇菜总黄酮的吸附性能最好

达48.0 mg·g-1湿树脂

AB-8 大孔树脂对天山堇菜总黄酮最佳洗脱浓度为35%乙醇

洗脱液为4 BV。天山堇菜总黄酮的得率达2.08%

纯度达71.1%。结论: 大孔树脂富集黄酮类化合物工艺简便

树脂再生容易

可用于工业化生产。

Abstract

Objective: To investigate the condition and parameters of adsorption and purification of total flavones contained in Viola tianshanica by macroporous resin so as to provide methods for the enrichment of flavonoids. Method: The adsorption properties of 3 kinds of macroporous resins for total flavonoids of V. tianshanica were compared; the yield and purity of total flavonoids from V. tianshanica were considered as standards

the purification process of total flavonoids in V. tianshanica by macroporous resin was selected. Result: It was found that theadsorption properties of AB-8 macroporous resins for total flavonoids of V. tianshanica were the best

up to 48 mg·g-1 wet resin

the best conditions to elute the total flavonoids adsorbed by AB-8 macroporous resin was 35% ethanol

resin vs. crude drug was 2.5: 1

ratio of diameter to height was 1:8.Using this process

the yield of the total flavones of V. tianshanica was up to 2.08%

the purity was 71.1%. Conclusion: This process is simple and practicable

it can be used to purify the total flavones contained in V. tianshanica.

关键词

Keywords

references

Views

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Studies on Purification of Saponins (PNS) with Macroporous Resin

Study on Separation and Purification Total Glycosides of Tree Peony Bark by Macroporous Resin

Purification of Total Alkaloid from Rhizoma Coptidis by Weakly Acidic Ion Exchange Resin

Related Author

LIU Zhong-qiu

CAI Xiong

LAI Xiao-ping

ZHU Chen-chen

LIU Liang

PAN Jun1

YU Qing-hua1

GUI Shuang-ying 1

Related Institution

School of Pharmacy,Shandong University of Traditional Chinese Medicine,Ji’nan

Zhejiang Chinese Medical University

School of Pharmacy，Tianjin University of Traditional Chinese Medicine

School of Pharmacy， Jiangxi University of Chinese Medicine

Institute of Chinese Materia Medica，China Academy of Chinese Medical Sciences

AI问答

Postal code：100700
Tel：010-84076882 Email：syfjx_2010@188.com
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备11006657号-10 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰