GC-MS Analysis of Volatile Constituents of

LI Ming; WANG Qiao-rong; LIU Jian-hua; HUANG Shun-ju; HUO Xin

doi:10.11653/syfj2013190122

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GC-MS Analysis of Volatile Constituents of

更新时间：2024-01-04

- GC-MS Analysis of Volatile Constituents of
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 19, Pages: 122-126(2013)
- 作者机构：
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- DOI：10.11653/syfj2013190122
  CLC：
- Published：2013
- 稿件说明：
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LI Ming, WANG Qiao-rong, LIU Jian-hua, et al. GC-MS Analysis of Volatile Constituents of [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(19): 122-126.
DOI：

LI Ming, WANG Qiao-rong, LIU Jian-hua, et al. GC-MS Analysis of Volatile Constituents of [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(19): 122-126. DOI： 10.11653/syfj2013190122.

摘要

目的: 分析望江南子Cassia occidentalis L.的挥发性成分

为药用植物望江南的开发利用提供实验依据。方法: 利用水蒸气蒸馏法提取望江南子挥发油

采用气相色谱-质谱联用(GC-MS)技术对挥发油进行分析。结果: 共分离出101个化学成分

鉴别出86个化学成分

占挥发油总量的90.07%

其主要成分为香叶基丙酮(16.84%);β-紫罗兰酮(11.68%);6-甲基-5-庚烯-2-酮(5.37%);叶绿醇(3.70%);6

14-三甲基-2-十五烷酮(3.67%);法尼基丙酮(3.36%);正己醛(3.12%);α-紫罗酮(3.12%)。结论: 采用气相色谱-质谱联用法对望江南子的挥发性成分进行研究

分离效果较好。

Abstract

Objective: To provide the foundation for reasonable utilization by analyzing the volatile constituents of Cassia occidentalis. Method: The volatile oil was extracted from C. occidentalis by team distillation. The chemical constituents were analyzed by GC-MS. Result: One hundred and one compounds were separated and eighty-six of them were identified

which accounted for 90.07% of all the volatile oil. The major components were geranylacetone (16.84%)

β-ionone (11.68%)

6-methyl-5-hepten-2-one (5.37%)

phytol (3.70%); 6

14-trimethyl-2-pentadecanone (3.67%)

farnesyl acetone (3.36%)

hexanal (3.12%)

α-ionone (3.12%). Conclusion: The volatile oil was extracted and analyzed from C. occidentalis by GC-MS.

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