Study on Chemical Constituents from

LIAN Lian; XIAN Xiao-yan; CHU Dong-hai; JIA Wei-li; GAO Hui-yuan

doi:10.11653/syfj2013190149

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Study on Chemical Constituents from

更新时间：2024-01-04

- Study on Chemical Constituents from
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 19, Pages: 149-152(2013)
- 作者机构：
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- DOI：10.11653/syfj2013190149
  CLC：
- Published：2013
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LIAN Lian, XIAN Xiao-yan, CHU Dong-hai, et al. Study on Chemical Constituents from [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(19): 149-152.
DOI：

LIAN Lian, XIAN Xiao-yan, CHU Dong-hai, et al. Study on Chemical Constituents from [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(19): 149-152. DOI： 10.11653/syfj2013190149.

摘要

目的: 对中药材川黄柏的化学成分进行研究。方法: 采用硅胶柱色谱、Sephadex LH-20、ODS柱色谱、制备型HPLC及重结晶等方法进行分离纯化

通过理化常数测定、光谱数据进行结构鉴定。结果: 从川黄柏的75%乙醇提取物中分离得到了11个化合物

分别鉴定为:小檗碱(berberine

1)、黄柏内酯(obaculactone

2)、石虎柠檬素A(shihulimonin A

3)、N-p-coumaroyltyramine(4)、1-(4-hydroxy-3-methoxyphenyl)-2-[4-(3-hydroxy-propyl)-2-methoxyphenoxy]-propane-1

3-diol(5)、黄柏碱(phellodendrine

6)、木兰花碱(magnoflorine

7)、巴马汀(palmatine

8)、药根碱(jatrorrhizine

9)、非洲防己碱(columbamine

10)、黄柏酮(obacunone

11)。结论: 化合物3

5为从黄檗属植物中首次分离得到

化合物4为从该种植物中首次分离得到。

Abstract

Objective: To isolate and identify chemical constituents from Phellodendron chinense. Method: Compounds were isolated by silica gel and Sephadex LH-20 column chromatography

and their structures were determined by means of the spectral analysis and physicochemical properties. Result: Eleven compounds were isolated and identified as berberine(1)

obaculactone(2)

shihulimoninA(3)

N-p-coumaroyltyramine(4)

1-(4-hydroxy-3-methoxyphenyl)-2-[4-(3-hydroxy-propyl)-2-methoxyphenoxy]-propane-1

3-diol(5)

phellodendrine(6)

magnoflorine(7)

palmatine(8)

jatrorrhizine (9)

columbamine (10)

obacunone (11). Conclusion: Compounds 3 and 5 were isolated from P. genus for the first time

and compound 4 was isolated from this plant for the first time.

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