YANG Fen-fang, HAO Zhi-hui, DING Zhao-peng. Study and Evaluation of Quality Control of Echinacea Purpurea Oral Liquid[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(20): 65-67.
DOI:
YANG Fen-fang, HAO Zhi-hui, DING Zhao-peng. Study and Evaluation of Quality Control of Echinacea Purpurea Oral Liquid[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(20): 65-67. DOI: 10.11653/syfj2013200065.
Study and Evaluation of Quality Control of Echinacea Purpurea Oral Liquid
Objective: To establish the quality standard and evaluation of Echinacea Purpurea oral liquid. Method: TLC test was based on silica gel plate with the upper solution of ethyl acetate-acetic acid-water (6:0.5:1) as mobile phase. The analytical column was Agilent Eclipse XDB-C18(4.6 mm×250 mm
5 μm) with acetonitrile and 0.3% phosphoric acid as mobile phase in gradient mode;the flow rate was 1.2 mL·min-1;the detecting wavelength was set at 330 nm;the column temperature was set at 35℃ and the injection volume was 10 μL. At the same time
pH and relative density were determined. Result: Characteristic of Echinacea Purpurea oral liquid was clear. The linear range of cichoric acid was 0.004-0.128 g·L-1(r=0.999 9)
and the average recovery was 101.13% with RSD 1.41%. Conclusion: The method to identify cichoric acid is simple and has a great repeatability. The method to detemine the content of cichoric acid in Echinacea Purpurea oral liquid is simple
accurate with a good reproducibility. So the TLC and HPLC methods can be used for the quality of the oral liquid.
Studies on Qualitative and Quantitative Methods of Liangge Pills
Studies on the Quality standard of Bimintong Capsule
Quality Standard Study for Kangan Liyan Capsule
Study on the Quality Standard of Licorice Juice as A Processing Excipient
Studies on Quality Control Standard of Modified Xileisan Suppository
Related Author
SHI Tao1
2
MENG Xian-sheng2
3
LUO Guo-an2
WANG Yi-ming2
GONG Qian-feng1
CHENG Yao-tang
Related Institution
Hubei Institute for Food and Drug Control
Gansu Province Hospital of Traditional Chinese Medicine
Acupuncture and Moxibustion Hospital Affiliated to Anhui College of Traditional Chinese Medicine & Anhui Modern Engineering Technology Research Center of Chinese Medicine