Determination of Ditro Dissolution of Suxiao Zhixie Capsule

MA Qi-wu; YANG Chang; LIU Qiu-yu; LIN Sen; WANG Dan-wei; MA Qi-zhen

doi:10.11653/syfj2013200108

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Determination of Ditro Dissolution of Suxiao Zhixie Capsule

更新时间：2024-01-04

- Determination of Ditro Dissolution of Suxiao Zhixie Capsule
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 20, Pages: 108-111(2013)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.11653/syfj2013200108
  CLC：
- Published：2013
- 稿件说明：
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MA Qi-wu, YANG Chang, LIU Qiu-yu, et al. Determination of Ditro Dissolution of Suxiao Zhixie Capsule[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(20): 108-111.
DOI：

MA Qi-wu, YANG Chang, LIU Qiu-yu, et al. Determination of Ditro Dissolution of Suxiao Zhixie Capsule[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(20): 108-111. DOI： 10.11653/syfj2013200108.

摘要

目的: 建立速效止泻胶囊体外溶出度测定方法

考察其体外溶出规律。方法: 采用高效液相色谱(HPLC)

检测波长256 nm

溶出介质为0.1 mol·L-1 HCl

转速120 r·min-1

浆法(沉降蓝)。结果: 速效止泻胶囊溶出率的均一性和重复性良好

以45 min为取样时间

盐酸小檗碱溶出率不少于75%为限度。结论: 方法简单、准确、可靠

可用于速效止泻胶囊溶出度的测定。

Abstract

Objective: This manuscript presents a method to research the dissolution and external leaching rule of Suxiao Zhixie capsule. Method: By using of HPLC method

the wavelength of the spectrophotometer set at 256 nm. The dissolution medium is 0.1 mol·L-1 HCl

the rotate speed is 120 r·min-1(settlement basket method). Result: We get a good uniform and repeatability during assaying the dissolution of Suxiao Zhixie capsule. The sampling time should be 45 min

and the percentage of dissolution should not less than 75%. Conclusion: The method we used to assay the dissolution of Suxiao Zhixie capsule is simple

accuracy and reliable.

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