Chemical Constituents from

LI Zhi-feng; WANG Qi; LIU Yan-ting; LI Xiang; OUYANG Sheng; FENG Yu-lin; YANG Shi-lin

doi:10.11653/syfj2013210056

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Chemical Constituents from

更新时间：2024-01-04

- Chemical Constituents from
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 21, Pages: 56-61(2013)
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- DOI：10.11653/syfj2013210056
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- Published：2013
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LI Zhi-feng, WANG Qi, LIU Yan-ting, et al. Chemical Constituents from[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(21): 56-61.
DOI：

LI Zhi-feng, WANG Qi, LIU Yan-ting, et al. Chemical Constituents from[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(21): 56-61. DOI： 10.11653/syfj2013210056.

摘要

目的: 研究预知子Akebia trifoliata 的化学成分。方法: 利用各种色谱技术进行分离

根据所得单体化学成分的理化性质与光谱数据鉴定其结构。结果: 从预知子中分离得到10个已知成分

分别鉴定为3-O-β-D-吡喃葡萄糖(1→3)-α-L-吡喃鼠李糖-(1→2)-α-L-吡喃阿拉伯糖-常春藤皂苷(1)

3-O-β-D-吡喃阿拉伯糖-(1→2)-α-L-吡喃阿拉伯糖-常春藤皂苷(2)

3-O-α-L-吡喃鼠李糖-(1→2)-α-L-吡喃阿拉伯糖-常春藤皂苷(3)

3-O-α-L-吡喃阿拉伯糖-常春藤皂苷 (4)

3-O-α-L-吡喃鼠李糖-(1→2)-α-L-吡喃阿拉伯糖-28-O-β-D-吡喃葡萄糖(1→6)-β-D-吡喃葡萄糖常春藤皂苷(5)

3-O-α-L-吡喃鼠李糖-(1→2)-[β-D-吡喃葡萄糖(1→4)]-α-L-吡喃阿拉伯糖-常春藤皂苷(6)

3-O-α-L-吡喃鼠李糖-(1→2)[β-D-吡喃葡萄糖(1→4)]-α-L-吡喃阿拉伯糖-28-O-α-吡喃鼠李糖-(1→4)-β-D-吡喃葡萄糖(1→6) 吡喃葡萄糖常春藤皂苷(7)

28-O-β-D-吡喃木糖(1→3)-O-α-L-吡喃鼠李糖-(1→2)-β-D-吡喃葡萄糖(1→6)-β-D-吡喃葡萄糖阿江榄仁酸皂苷 (8)

28-O-α-L-吡喃鼠李糖-(1→4)-O-β-D-吡喃葡萄糖-(1→6)-O-β-D-吡喃葡萄糖去甲阿江榄仁酸皂苷 (9)

3-O-β-D-α-L-吡喃鼠李糖-(1→2)-α-L-吡喃阿拉伯糖-28-O-β-D-吡喃葡萄糖常春藤皂苷(10)。结论: 化合物8

9为首次从该植物中分离得到

化合物10为首次从该属植物中分离得到。

Abstract

Objective: To study the chemical constituents of Akebia trifoliata.Method: The compounds were separated and purified by column chromatography and their structures were established by spectroscopic methods. Result: Fifteen compounds were isolated from the extract of A. trifoliata

whose structures were determined as 3-O-β-D-glucopyranosyl(1→3)-α-L-rhamnopyranosyl-(1→2)-α-L-arabinopyranosyl hederagenin(1)

3-O-β-D-xylopyranosyl-(1→2)-α-L-arabinopyranosyl hederagenin(2)

3-O-α-L-rhamnopyranosyl-(1→2)-α-L-arabinopyranosyl hederagenin(3)

3-O-α-L-arabinopyranosidehederagenin(4)

3-O-α-L-rhamnopyranosyl(1→2)-α-L-arabinopyranosyl-28-O-β-D-glucopyranosyl(1→6)-β-D-glucopyranoside hederagenin(5)

3-O-([β-D-glucopyranosyl(1→4)]-[α-L-rhamnopyranosyl-(1→2)]-α-L-arabinopyranosyl)hederagenin(6)

3-O-α-L-rhamnopyranosyl(1→2)-[β-D-glucopyranosyl(1→4)]-α-L-arabinopyranosyl-28-O-α-L-rhamnopy-ranosyl-(1→4)-β-D-glucopyranosyl(1→6)-β-D-glucopyra-nosidehederagenin(7)

28-O-β-D-xylopyranosyl-(1→3)-O-α-L-rhamnopyranosyl-(1→2)-β-D- glucopyranosyl (1→6)-β-D-glucopyranoside arjunolic acid (8)

28-O-α-L-rhamnopyranosyl-(1→2)-β-D-glucopyranosyl (1→6)-β-D-glucopyranoside 30-no arjunolic acid (9)

3-O-α-L-rhamnopyranosyl(1→2)-α-Larabinopyranosyl-28-O-β-D-glucopyranosi-de hederagenin (10). Conclusion: Compounds 8

9 were isolated from this plant for the first time and 10 was isolated from genus acanthopanax for the first time.

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