Content Determination of Four Reference Ingredients in Refined Extract Solution of ARPD

CHEN Bu-you; OU Yao; LI Shu-guang; XIAO Ming-bing; JIANG Feng; ZHOU Shi-zhong; QIAN Xia; GU Hong-mei; LU Ya-peng

doi:10.11653/syfj2013210141

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Content Determination of Four Reference Ingredients in Refined Extract Solution of ARPD

更新时间：2024-01-04

- Content Determination of Four Reference Ingredients in Refined Extract Solution of ARPD
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 21, Pages: 141-144(2013)
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- DOI：10.11653/syfj2013210141
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- Published：2013
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CHEN Bu-you, OU Yao, LI Shu-guang, et al. Content Determination of Four Reference Ingredients in Refined Extract Solution of ARPD[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(21): 141-144.
DOI：

CHEN Bu-you, OU Yao, LI Shu-guang, et al. Content Determination of Four Reference Ingredients in Refined Extract Solution of ARPD[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(21): 141-144. DOI： 10.11653/syfj2013210141.

摘要

目的: 建立抗放射性肺炎方(anti-radiation pneumonia decoction

ARPD)精制液中4个指标成分的定量分析方法。方法: 以芍药苷、阿魏酸、咖啡酸、甘草酸为考察指标

采用岛津LC-20AD系列高效液相色谱仪和Kromasil C18色谱柱(4.6 mm×250 mm

5 μm)

流动相乙腈-0.1% 磷酸

进行梯度洗脱

流速1.0 mL·min-1

柱温30 ℃。结果: ARPD精制液中芍药苷、阿魏酸、咖啡酸和甘草酸的质量浓度分别为522

143 mg·L-1。结论: 各指标成分检测方法的稳定性、准确度和回收率良好

可用于ARPD精制液的质量控制。

Abstract

Objective: To establish the analytical method of quality control for the four reference ingredients in anti-radiation pneumonia decoction (ARPD). Method: Herbaceous peony glucoside

ferulic acid

coffee acid and glycyrrhizic acid were adopted as the reference substances. HPLC method was established using SHIMADZU LC-20AD HPLC system. Kromasil C18 column (4.6 mm×250 mm

5 μm) was used at 30 ℃. Mobile phase consisted of acetonitrile-0.1% phosphoric acid was used for gradient elution at a flow rate of 1.0 mL·min-1. Result: The contents of herbaceous peony glucoside

ferulic acid

coffee acid and glycyrrhizic acid in ARPD refined extract were 522

143 mg·L-1

respectively. Conclusion: The stability

accuracy and recovery of the methods are good and can be used for the quality control of ARPD refined extract.

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