ZHANG Ying, CUI Wen, KANG Ze-feng. Quality Standards of Mushu Pills[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(22): 67-70.
DOI:
ZHANG Ying, CUI Wen, KANG Ze-feng. Quality Standards of Mushu Pills[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(22): 67-70. DOI: 10.11653/syfj2013220067.
Objective: To develop the qualitative and quantitative methods for quality control of Mushu pills. Method: TLC were used as qualitative identifications of Paeoniae Radix Alba and Corydalis Rhizoma in Mushu pills;And to develop a HPLC method for determination of paeoniflorin in Mushu pills
separation was performed on ZORBAX SB-C18 column(4.6 mm×150 mm
5μm)with acetonitrile-0.1% phosphoric acid(15: 85) as mobile phase
flow rate of 1.0 mL·min-1
detection wavelength was at 230 nm
injection volume 10 μL
column temperature was 30 ℃. Result: TLC characteristic identification was distinct and highly specific.Paeoniflorin showed a good liner relationship within the range of 37.80-756.00 ng
the average recovery was 98.2% with RSD 1.4%. Conclusion: This established determination method was reliable
accurate and specific
it could be used for quality control of Mushu pills.
Optimization of Processing Technology for Paeoniae Radix Alba with Terra Flava Usta by Response Surface-central Composite Test
Studies on Quality Standard for Danqi Quyu Zhitong Granules
Simultaneous Determination of Paeoniflorin, Salvianolic Acid B and Berberine in Fuyankang Pills by HPLC
HPLC Analysis of the Composition of Albiflorin, Paeoniflorin, 2,3,5,4'-Tetrahydro Xystilbene-2--Glucoside and Penta--Galloyl--Glucoside in Kundan Capsule
Optimization of Smashing Tissue Extraction Process of Total Paeony Glycoside by Orthogonal Test
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