JIANG Yun-bin, LU Xiao-lin, YANG Zhi-zhong, et al. Studies on the Chemical Constituents of Related to Sulfur Fumigated[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(22): 74-78.
DOI:
JIANG Yun-bin, LU Xiao-lin, YANG Zhi-zhong, et al. Studies on the Chemical Constituents of Related to Sulfur Fumigated[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(22): 74-78. DOI: 10.11653/syfj2013220074.
Studies on the Chemical Constituents of Related to Sulfur Fumigated
Objective: To find the correlative characteristic components of Angelicae Dahuricae Radix which is related to sulfur fumigated. Method: Normal or reversed phase partition chromatography
mass spectrum and nuclear magnetic resonance spectroscopy were used for isolation and identification of compounds. Using high-performance liquid chromatography(HPLC) analysised. Result: Thirteen compounds were obtained and identified as oxypeucedanin(1)
phellopterin(2)
xanthotoxin(3)
oxypeucedanin hydrate(4)
pabulenol(5)
marmesin(6)
byakangelicin(7)
bergapten(8)
isopimpinellin(9)
imperatorin(10)
isoimperatorin(11)
byakangelicol(12) and neobyakangelicol(13). Oxypeucedanin
oxypeucedanin hydrate
bergapten and byakangelicol were obviously changed in HPLC fringerprints after fumigated with sulfur. Conclusion: The quality control of Angelicae Dahuricae Radix provide new evidence for the selection of indicators.