Analysis of Procymidone Residues in Ginseng Extract by HPLC

REN Gang; LIAO Wei-bo; HU Zhi-cheng; YI Wen-fang; LIU Rong-hua; SHAO Feng; HUANG Hui-lian; YUAN Jin-bin

doi:10.11653/syfj2013230107

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Analysis of Procymidone Residues in Ginseng Extract by HPLC

更新时间：2024-01-04

- Analysis of Procymidone Residues in Ginseng Extract by HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 23, Pages: 107-110(2013)
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- DOI：10.11653/syfj2013230107
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- Published：2013
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REN Gang, LIAO Wei-bo, HU Zhi-cheng, et al. Analysis of Procymidone Residues in Ginseng Extract by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(23): 107-110.
DOI：

REN Gang, LIAO Wei-bo, HU Zhi-cheng, et al. Analysis of Procymidone Residues in Ginseng Extract by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(23): 107-110. DOI： 10.11653/syfj2013230107.

摘要

目的: 建立人参提取物中农药残留-腐霉利的HPLC含量测定方法。方法: BDS HYPERSIL C18分析色谱柱（4.6 mm×250 mm，5 μm），流动相乙腈-水（40∶60），流速1.0 mL·min-1，检测波长220 nm。结果: 腐霉利进样量0.001~0.6 μg与色谱峰面积呈良好线性关系（R2=0.999 4），平均加样回收率100.0%（n=9），RSD 3.0%。结论: 该法简便、准确、可靠，可用于人参提取物中腐霉利残留的含量测定。

Abstract

Objective: To establish a HPLC method for the determination of procymidone residues in ginseng extract. Method: The BDS HYPERSIL C18 (4.6 mm×250 mm

5 μm) column was used as analytical column with the mobile phase of acetonitrile-water (40:60) at the flow rate of 1.0 mL· min-1

and the detective wavelength was set at 220 nm. Result: Good linear range was obtained for the procymidione with an injection amount ranging from 0.001 to 0.6 μg (R2=0.999 4). The average recovery was 100.0% (n=9)

and RSD was 3.0%. Conclusion: The HPLC method is simple

accurate and effective

which can be used for the detection of procymidone pesticide residues in ginseng extract.

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