Chemical Constituents Analysis of Volatile Oil in Arthritis Powder of Qiang Medicine by GC-MS

SHENG Fei-ya; FU Chao-mei; HU Hui-ling; LIN Jun-zhi; LI Ying; BAO Xi-fu

doi:10.11653/syfj2014010087

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Chemical Constituents Analysis of Volatile Oil in Arthritis Powder of Qiang Medicine by GC-MS

更新时间：2024-01-04

- Chemical Constituents Analysis of Volatile Oil in Arthritis Powder of Qiang Medicine by GC-MS
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 20, Issue 1, Pages: 87-90(2014)
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- DOI：10.11653/syfj2014010087
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- Published：2014
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SHENG Fei-ya, FU Chao-mei, HU Hui-ling, et al. Chemical Constituents Analysis of Volatile Oil in Arthritis Powder of Qiang Medicine by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(1): 87-90.
DOI：

SHENG Fei-ya, FU Chao-mei, HU Hui-ling, et al. Chemical Constituents Analysis of Volatile Oil in Arthritis Powder of Qiang Medicine by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(1): 87-90. DOI： 10.11653/syfj2014010087.

摘要

目的：用气相色谱-质谱联用（GC-MS）技术分离鉴定羌药关节炎散挥发油的化学成分。方法：水蒸气蒸馏法提取关节炎散挥发油，采用GC-MS法分离鉴定，用面积归一法测定各化合物相对含量。结果：共分离鉴定了33个化学成分，占总成分相对含量的86.47%，其中相对含量超过5%的成分有丹皮酚（13.20%）、芳樟醇（10.94%）、白菖烯（9.48%）、枞油烯（7.93%）、2-亚甲基-6，8，8，-三甲基-三环[5.2.2.0（1，6）]十一碳-3-醇（5.01%）。结论：可为关节炎散的质量控制和进一步药效研究提供一定的参考。

Abstract

Objective: To analyze the chemical constituents of the volatile oil from arthritis powder of Qiang medicine by GC-MS. Method: The water distillation was used to extract the volatile oil

GC-MS technology was used to analyze the components of the volatile oil

and area normalization was used to determine the relative content of each component. Result: Thirty-three chemical components were identified

which was 86.47% of total components. The relative amounts of 5 components were above 5%. They were paeonol (13.20%)

linalool (10.94%)

(+)-calarene (9.48%)

sylvestrene (7.93%)

tricyclo [5.2.2.0(1

6)] undecan-3-ol

2-methylene-6

8-trimethyl-(5.01%). Conclusion: The experiment provides some evidence of quality control and further pharmacodynamics study foundation of arthritis powder.

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