UPLC Fingerprint Analysis and Pattern Recognition of

LIU Jing; SU Jian-chun; GAN Lin-jian; YIN Rong-li; LI Hua

doi:10.11653/syfj2014040087

您当前的位置：

首页 >

文章列表页 >

UPLC Fingerprint Analysis and Pattern Recognition of

更新时间：2024-01-04

- UPLC Fingerprint Analysis and Pattern Recognition of
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 20, Issue 4, Pages: 87-90(2014)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.11653/syfj2014040087
  CLC：
- Published：2014
- 稿件说明：
移动端阅览
LIU Jing, SU Jian-chun, GAN Lin-jian, et al. UPLC Fingerprint Analysis and Pattern Recognition of [J]. Chinese journal of experimental traditional medical formulae, 2014, 20(4): 87-90.
DOI：

LIU Jing, SU Jian-chun, GAN Lin-jian, et al. UPLC Fingerprint Analysis and Pattern Recognition of [J]. Chinese journal of experimental traditional medical formulae, 2014, 20(4): 87-90. DOI： 10.11653/syfj2014040087.

摘要

目的：建立鸡血藤药材UPLC指纹图谱方法。方法：采用UPLC-DAD检测，以甲醇-0.1%甲酸为流动相，进行梯度洗脱。色谱柱为Aquity BEH C18（2.1 mm×50 mm，1.7 μm），检测波长280 nm，柱温30 ℃，流速0.4 mL·min-1。采用用聚类分析和主成分分析对18批鸡血藤指纹图谱进行模式识别研究。结果：筛选出10批样品建立了鸡血藤指纹图谱的共有模式。结论：该方法为鸡血藤药材的质量控制提供了一种快速、简便和全面的评价方法。

Abstract

Objective: To establish the fingerprint of Spatholobus suberectus by UPLC. Method: The UPLC-DAD method was performed on Aquity BEH C18 (2.1 mm×50 mm

1.7 μm)column with the gradient mobile phase of methanol (A) and 0.1% formic acid (B) solution at flow rate of 0.4 mL·min-1. The detection wavelength was set at 280 nm. The column temperature was 30 ℃. Eighteen samples from various places were analyzed.Clusters analysis and principal component analysis(PCA) were applied to study the chemical pattern recognition of UPLC fingerprints. Result: Ten samples were selected to establish the common pattern of S. suberectus. Conclusion: The method provides a fast

simple and comprehensive method for the quality control of S. suberectus.

关键词

Keywords

references

Views

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Investigation of UPLC Fingerprint for Kangfuxin Liquid

HPLC Fingerprint Analysis of Substance Benchmark of Xiao Chengqitang

Improvement of Quality Standard of Shenwei Gubi Tablets and Changes of Transfer Rates of Its Quality Control Indicators in Production Based on Chemical Pattern Recognition Technology

Spectrum-effect Relationship of Anti-hepatoma Activity from 3 Kinds of Genus Paris Based on Cluster Analysis and Grey Relational Analysis

Changes of HPLC Fingerprint and Main Flavonoids Content of Aurantii Fructus Before and After Processing

Related Author

WU Hong-mei

XU Feng

LIU Li-mei

WANG Xiang-pei

YANG Ming

Yan MENG

Wu-yi LI

Jia-ming SHAN

Related Institution

Key Laboratory of Modern Preparation of Traditional Chinese Medicine （TCM），Ministry of Education，Jiangxi University of TCM

Kunming Municipal Hospital of Traditional Chinese Medicine

Yunnan Provincial Key Laboratory of Research on External Drug Delivery System and Preparation Technology in University，Yunnan University of Chinese Medicine

College of Pharmacy and Chemistry, Key Laboratory of Universities in Yunnan Province on Development of Genuine Medicinal Materials Resources in Western Yunnan, Dali University

The First People's Hospital of Yiliang

AI问答

Postal code：100700
Tel：010-84076882 Email：syfjx_2010@188.com
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备11006657号-10 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰