Studies on Chemical Constituents of

LI Tao; BAI Hong; ZHONG Hao; DENG Zhi-peng; YAO Qing-qiang

doi:10.11653/zgsyfjxzz2013070140

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Studies on Chemical Constituents of

更新时间：2024-01-04

- Studies on Chemical Constituents of
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 7, Pages: 140-143(2013)
- 作者机构：
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- DOI：10.11653/zgsyfjxzz2013070140
  CLC：
- Published：2013
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LI Tao, BAI Hong, ZHONG Hao, et al. Studies on Chemical Constituents of [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(7): 140-143.
DOI：

LI Tao, BAI Hong, ZHONG Hao, et al. Studies on Chemical Constituents of [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(7): 140-143. DOI： 10.11653/zgsyfjxzz2013070140.

摘要

目的: 对毛果一枝黄花Solidago virgaurea的化学成分进行研究。方法: 采用硅胶柱色谱

凝胶柱色谱

ODS反相柱色谱以及重结晶等方法分离纯化

并通过理化常数和波谱分析鉴定化合物结构。结果: 分离并鉴定出了12个化合物

分别为2'-甲氧基-2-甲氧基-6-羟基苯甲酸酯(1)

2'-甲氧基-2

6-二甲氧基苯甲酸酯(2)

β-乙酰香树脂醇乙酸酯(3)

α-菠菜甾醇(4)

豆甾-7

22-二烯-3-酮(5)

2-羟基-6-甲氧基苯甲酸(6)

胡麻素(7)

槲皮素(8)

山奈酚(9)

3β-acetoxyolean-12-en-11-one-acetate(10)和N-benzoylphenylalaninyl-N-benzoylphenylalaninate(11)

原儿茶酸(12)。结论: 化合物11为首次从该科植物中分离得到

化合物5

10为该属内首次分离

化合物1

12为首次从该植物中分离得到。

Abstract

Objective: To Study the chemical constituents of the Solidago virgaurea. Method: The compounds were isolated and purified from the plant with chromatography techniques and the structures were identified on the basis of spectral analyses and physicochemical properties. Result: Twelve compounds were isolated from S. virgaurea and their structures were identified as 2'-methoxybenzyl-2-methoxy-6-hydroxybenzoate

2'-methoxybenzyl-2

6-dimetho-xybenzoate

β-amyrin acetate

α-spinasterol

stigmasta-7

22-dien-3-one

hexadecanoic acid

2-hydroxy-6-methoxybenzoic acid

pedalitin

quercecetin

kaemferol

3β-acetoxyolean-12-en-11-one-acetate

N-benzoylphenylalaninyl-N-benzoylphenylalaninate and protocatechoic acid. Conclusion: Compounds 11 was isolated from Solidago for the first time

compounds 5 and 10 were isolated from Solidago genus for the first time

compounds 1

7 and 12 were isolated from the plant for the first time.

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Related Institution

School of Pharmacy, Jiangxi University of Traditional Chinese Medicine(TCM)

Graduate School, Jiangxi University of TCM

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