Analysis of Fatty Acid of Fruits of with GC-MS

XU Hui-wang; WU Jun; CHENG Fan; ZOU Kun; ZHOU Yuan

doi:10.11653/zgsyfjxzz2013070144

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Analysis of Fatty Acid of Fruits of with GC-MS

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- Analysis of Fatty Acid of Fruits of with GC-MS
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 7, Pages: 144-146(2013)
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- DOI：10.11653/zgsyfjxzz2013070144
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- Published：2013
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XU Hui-wang, WU Jun, CHENG Fan, et al. Analysis of Fatty Acid of Fruits of with GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(7): 144-146.
DOI：

XU Hui-wang, WU Jun, CHENG Fan, et al. Analysis of Fatty Acid of Fruits of with GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(7): 144-146. DOI： 10.11653/zgsyfjxzz2013070144.

摘要

目的: 分析木果楝Xylocarpus granatum果实中脂肪酸成分及相对含量。方法: 采用气相色谱-质谱联用技术

对木果楝果实中的脂肪酸以甲醇回流提取

石油醚萃取

硫酸甲醇甲酯化后进行测定

用面积归一化法得出各脂肪酸的相对含量。结果: 从木果楝中检出6种饱和脂肪酸和5种不饱和脂肪酸。其中饱和脂肪酸占总含量的17.63%

以棕榈酸含量最高(相对含量13.36%);不饱和脂肪酸占总含量的81.97%

以亚麻酸含量最高(相对含量73.86%)。结论: 为木果楝的药用价值开发提供了科学依据。

Abstract

Objective: To study the fatty acids of fruits of Xylocarpus granatum. Method: The gas chromatography and mass spectrometry was used in the study. The fatty acids of fruits of X. granatum were extracted by refluxing with anhydrous methanol and were abstracted with petroleum ether and were esterified with sulfuric acid-methanol. Result: In fruits of X. granatum

were detected to have eleven kinds of fatty acids. There were five kinds of unsaturated acids and the total amount were 81.97%.Respectively

the relative content of 9

15-octadecatrienoic acid was the highest. Conclusion: This study may provide scientific reference for the pharmacological use of X. granatum.

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