Analysis of Volatile Compounds from  with Solid Phase Microextraction by GC-MS

QIAN Zong-yao; AN Ran; HUA Zhen-yu; LI Jing; WANG Cheng

doi:10.13422/j.cnki.syfix.2014070082

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Analysis of Volatile Compounds from with Solid Phase Microextraction by GC-MS

更新时间：2024-01-04

- Analysis of Volatile Compounds from with Solid Phase Microextraction by GC-MS
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 20, Issue 7, Pages: 82-85(2014)
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- DOI：10.13422/j.cnki.syfix.2014070082
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- Published：2014
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QIAN Zong-yao, AN Ran, HUA Zhen-yu, et al. Analysis of Volatile Compounds from with Solid Phase Microextraction by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(7): 82-85.
DOI：

QIAN Zong-yao, AN Ran, HUA Zhen-yu, et al. Analysis of Volatile Compounds from with Solid Phase Microextraction by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(7): 82-85. DOI： 10.13422/j.cnki.syfix.2014070082.

摘要

目的：建立新疆雪菊挥发性成分的分析方法，鉴定其化学成分。方法：利用顶空固相微萃取技术（HS-SPME）吸附新疆雪菊中的挥发性成分。方法：色谱-质谱联用技术（GC-MS）分析鉴定，并用峰面积进行归一化定量。结果：从雪菊中共分离出54个峰，鉴定出其中的47种化学成分，占总峰面积的95.88%。雪菊中主要挥发性成分为3-蒈烯、1，3，8-对-薄荷三烯、α-柠檬烯、马鞭草烯醇、香芹酮等。结论：建立的方法分离度好，准确、可靠，为新疆雪菊挥发性成分的研究提供了分析方法。

Abstract

Objective: To identify the volatile compounds in Coriopsis ticntoria. Method: Volatile compounds from C. ticntoria were isolated by headspace solid phase microextraction (HS-SPME) and identified and quantified by gas chromatography-mass spectrometry (GC-MS). A quantitative analysis in percent was performed by peak area normalization measurements. Fifty-four peaks in C. ticntoria were detected respectively. Species of chemical componens were identified by GC-MS. Result: The content of the identified compounds extracted from C. ticntoria was 95.88% of the total volatile substances

3-carene

8-p-menthatriene

D-limonene

verbenol

carvone were the most abundant volatile compounds released from C. ticntoria. Conclusion: The method is simple

rapid and sensitive

which could be used for determination of volatile compounds in C. ticntoria.

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