Studies on Quality Control Standard of   Jiuweiqianghuo Concentrated Pills

QIN Chun-mei; LIU You-ping; YAN dan; CHEN Hong-ping

doi:10.13422/j.cnki.syfjx.2003.05.001

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Studies on Quality Control Standard of Jiuweiqianghuo Concentrated Pills

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- Studies on Quality Control Standard of Jiuweiqianghuo Concentrated Pills
- Chinese Journal of Experimental Traditional Medical Formulae Issue 5, Pages: 1-3(2003)
- 作者机构：
  
  1. 成都中医药大学
  2. 成都中医药大学四川成都610075
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2003.05.001
  CLC： R286.0
- Published：2003
- 稿件说明：
移动端阅览
[1]秦春梅,刘友平,鄢丹,陈鸿平.九味羌活丸(浓缩丸)质量标准研究[J].中国实验方剂学杂志,2003(05):1-3.

QIN Chun-mei, LIU You-ping, YAN dan, et al. Studies on Quality Control Standard of Jiuweiqianghuo Concentrated Pills[J]. Chinese journal of experimental traditional medical formulae, 2003, (5): 1-3.
[1]秦春梅,刘友平,鄢丹,陈鸿平.九味羌活丸(浓缩丸)质量标准研究[J].中国实验方剂学杂志,2003(05):1-3. DOI： 10.13422/j.cnki.syfjx.2003.05.001.

QIN Chun-mei, LIU You-ping, YAN dan, et al. Studies on Quality Control Standard of Jiuweiqianghuo Concentrated Pills[J]. Chinese journal of experimental traditional medical formulae, 2003, (5): 1-3. DOI： 10.13422/j.cnki.syfjx.2003.05.001.

摘要

目的 :建立九味羌活丸（浓缩丸）的质量标准。方法 :用TLC对处方中的苍术、黄芩、川芎进行定性鉴别 ;用HPLC法测定黄芩中黄芩苷的含量。结果 :TLC色谱能检出苍术、黄芩、川芎 ;黄芩苷的含量在 0 0 30 4～ 0 2 12 8μg范围内

与峰面积积分值呈良好的线性关系

r=0 9999

平均回收率 99 6 %

RSD =3 7%。结论 :所建立的方法能准确、快速地进行定性、定量检测

可用于九味浓缩丸的质量控制。

Abstract

Objective:To establish the quality control standard of Jiuweiqianghuo Concentrated Pills.Methods:Applying TLC to indentify Rhizoma atractylodis、Rhizoma Chuangxiong and Radix Scutellariae

Using HPLC to determine the content of baicalin of Radix Scutellariae.Results:Rhizoma atractylodis、Rhizoma Chuangxiong and Radix Scutellariae could be indentified by TLC;baicalin showed a good linear relationship at the rang of 0.0304～0.2128μg

r0.9999.The average recovery was 99.6%

and RSD was 3.7%.Conclusion:The methods are accurate and quick

and can be used for the quality control of Jiuweiqianghuo Concentrated Pills.

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Related Author

QIN Chun-mei

LIU You-ping

YAN dan

CHEN Hong-ping

LI Jun-jiang

ZHANG Bing-sheng1

WANG Peng-yi2

WANG Rui-fen3

Related Institution

Research Center for Differentiation and Development of Traditional Chinese Medicine （TCM） Basic Theory， Jiangxi Province Key Laboratory of TCM Etiopathogenisis， Jiangxi University of Chinese Medicine

Henan Academy of Chinese Medicine

The Second Clinical Medical College， Henan University of Chinese Medicine

State Key Laboratory of Functions and Applications of Medicinal Plants，School of Pharmaceutical Sciences，Engineering Center of Microbiology and Biochemical Pharmacy，Experimental Animal Center，Guizhou Medical University

Chengdu University of Traditional Chinese Medicine

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