RP-HPLC Determination of Kaempferide in Fuyang Tablets

FU Hui-zheng~

doi:10.13422/j.cnki.syfjx.2008.01.013

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RP-HPLC Determination of Kaempferide in Fuyang Tablets

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- RP-HPLC Determination of Kaempferide in Fuyang Tablets
- Chinese Journal of Experimental Traditional Medical Formulae Issue 1, Pages: 8-9(2008)
- 作者机构：
  
  1. 江西中医学院
  2. 江西省食品药品检验所
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2008.01.013
  CLC： R286
- Published：2008
- 稿件说明：
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[1]付辉政,万凯化,罗跃华.RP-HPLC法测定肤痒片中山柰素的含量[J].中国实验方剂学杂志,2008(01):8-9.

FU Hui-zheng~. RP-HPLC Determination of Kaempferide in Fuyang Tablets[J]. Chinese journal of experimental traditional medical formulae, 2008, (1): 8-9.
[1]付辉政,万凯化,罗跃华.RP-HPLC法测定肤痒片中山柰素的含量[J].中国实验方剂学杂志,2008(01):8-9. DOI： 10.13422/j.cnki.syfjx.2008.01.013.

FU Hui-zheng~. RP-HPLC Determination of Kaempferide in Fuyang Tablets[J]. Chinese journal of experimental traditional medical formulae, 2008, (1): 8-9. DOI： 10.13422/j.cnki.syfjx.2008.01.013.

摘要

目的:建立肤痒片中山柰素的含量测定方法。方法:用Diamonsil C18色谱柱（4.6 mm×250 mm

5μm）

以甲醇-0.4%磷酸溶液（58∶42）

流速为1.0 mL·min-1

检测波长为367 nm。结果:山柰素在（0.041

.41）μg范围内呈良好的线性关系

平均回收率和RSD分别为99.1%和1.1%。结论:本方法简便、准确、重现性好

可作为该制剂的含量测定方法。

Abstract

Objective:To develop a RP-HPLC method for determination of kaempferide in Fuyang Tablets.Methods:Diamonsil C

column（4.6 mm×250 mm

5 μm）was used

methanol-0.4% phosphoric acid solution（58∶42）as the mobile phase

flow rate at 1.0 mL·min

-1

and the detection wavelength was 367 nm.Results: The calibration curves were linear between（0.041～0.41）μg

The average recovery and the relative standard deviations were 99.1% and1.1%.Conclusions: The method is simple

accurate

repeatable and could be used for determination of kaempferide in the preparation.

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Related Author

FU Hui-zheng1

WAN Kai-hua2

LUO Yue-hua2

WAN Kai-hua1

FU Hui-zheng2

LUO Yong-ming2

ZHANG Dong-ming3

LIU Yan

Related Institution

College of Pharmacy, Gansu University of Chinese Medicine

Gansu Province Key Laboratory of Pharmacology and Toxicology of Traditional Chinese Medicine

Gansu Provincial Hospital

Guangzhou University of Chinese Medicine

Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences

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