Studies on Water-soluble substances and Determination of Danshensu and protocatechualdehyde of Herba Salvia chinensis

KANG Chen1; LI Man-ling1; WANG Qian1; HUANG Lu-qi1; Franco Francesco Vincieri2; Anna Rita Bilia2

doi:10.13422/j.cnki.syfjx.2009.07.012

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Studies on Water-soluble substances and Determination of Danshensu and protocatechualdehyde of Herba Salvia chinensis

更新时间：2024-09-23

- Studies on Water-soluble substances and Determination of Danshensu and protocatechualdehyde of Herba Salvia chinensis
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 15, Issue 7, Pages: 1-3(2009)
- 作者机构：
  
  1. 中国中医科学院中药研究所
  2. 意大利佛罗伦萨大学
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2009.07.012
  CLC： R284.1
- Published：2009
- 稿件说明：
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[1]康琛,李曼玲,王谦,黄璐琦,Franco Francesco Vincieri,Anna Rita Bilia.石见穿化学成分的提取分离及定量分析[J].中国实验方剂学杂志,2009,15(07):1-3.

KANG Chen1, LI Man-ling1, WANG Qian1, et al. Studies on Water-soluble substances and Determination of Danshensu and protocatechualdehyde of Herba Salvia chinensis[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(7): 1-3.
[1]康琛,李曼玲,王谦,黄璐琦,Franco Francesco Vincieri,Anna Rita Bilia.石见穿化学成分的提取分离及定量分析[J].中国实验方剂学杂志,2009,15(07):1-3. DOI： 10.13422/j.cnki.syfjx.2009.07.012.

KANG Chen1, LI Man-ling1, WANG Qian1, et al. Studies on Water-soluble substances and Determination of Danshensu and protocatechualdehyde of Herba Salvia chinensis[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(7): 1-3. DOI： 10.13422/j.cnki.syfjx.2009.07.012.

摘要

目的:研究石见穿全草的水溶性化学成分及进行含量分析。方法:利用水提、有机溶剂萃取及采用葡聚糖凝胶LH-20柱进行分离纯化

采用HPLC进行定量分析;结果:从石见穿水提取物中分得丹参素和迷迭香酸。HPLC色谱条件下

丹参素进样量在1.48～7.40μg范围内与峰面积积分值呈良好线性关系（r=0.999 9）

丹参素加样回收率（按丹参素钠计算）平均值为102.8%

RSD=1.04%;原儿茶醛进样量在0.05～0.26μg范围内与峰面积积分值呈良好线性关系（r=0.999 9）

原儿茶醛加样回收率平均值为101.5%

RSD=0.72%。结论:为石见穿的质量控制提供了可靠的检测方法。丹参素为首次从该植物中分离得到。

Abstract

Objective: To study and determine the Water-soluble substances of Salvia chinensis.Methods: The constituents of the n-Butanol-soluble portion of the water extractive were isolated and purified by means of Sephadex LH-20 column chromatographic methods.HPLC was used to determine the contents.Results: Two compounds were isolated and identified as danshensu and rosmarinic acid.The linear range of danshensu was 1.48～7.40 μg.The average recovery was 102.8% and RSD was 1.04%;The linear range of protocatechualdehyde was 0.05～0.26μg.The average recovery was 101.5% and RSD was 0.72%.Conclusion: The method can provide useful references to quality control of Herba Salvia chinensis.Danshensu was firstly isolated from Herba Salvia chinensis.

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Related Author

KANG Chen1

LI Man-ling1

Wang Qian1

HUANG Lu-qi1

Franco Francesco Vincieri2

Anna Rita Bilia2

Li-hong ZHOU

Feng-lian ZHANG

Related Institution

National & Local United Engineering Laboratory for TCM Advanced Manufacturing Technology, Tasly Pharmaceutical Co. Ltd.

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Institute of Traditional Chinese Medicine， Heilongjiang University of Chinese Medicine

Graduate School，Heilongjiang University of Chinese Medicine

Shandong University of Traditional Chinese Medicine

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