ZHANG Yan, JIN Xiang-qun, WANG Guang-shu. Studies on Qualitative and Quantitative Method of Gubaoxinshen Tablets[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(7): 14-16.
ZHANG Yan, JIN Xiang-qun, WANG Guang-shu. Studies on Qualitative and Quantitative Method of Gubaoxinshen Tablets[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(7): 14-16. DOI: 10.13422/j.cnki.syfjx.2009.07.017.
Studies on Qualitative and Quantitative Method of Gubaoxinshen Tablets
摘要
目的:制定骨宝昕肾片质量标准。方法:采用薄层色谱法鉴别大豆、淫羊藿
高效液相色谱法测定染料木素、淫羊藿苷的含量。结果:薄层斑点清晰
重现性好
染料木素的平均回收率为98.9%
RSD为0.9%;淫羊藿苷的平均回收率为98.0%
RSD为1.0%。结论:方法简便
准确
可供该品质量控制。
Abstract
Objective:To establish the qualitative and quantitative methods for Gubaoxinshen Tablets.Method: Soy bean
and epimedium herb were identified by TLC
and the content of genistein and icarrin were determined by HPLC.Result: The developed TLC sports were was fairly clear
the HPLC method showed good repeatability.The average recovery of genistein was 98.9% with RSD 0.9%
and the average recovery of icarrin the was 98.0% with RSD 1.0%.Conclusion: The method is simple
accurate and can becauseofon control quality of Gubaoxinshen Tablets.