Relativity between the Contents of Five Anthraquinones and the Appearance of Rhubarb Produced in Quanshui Village

DAI Wan-ying~1; SUN Wei-hong~2; MAO Shu-jie~1; GU Xue-zhu~1; NIU Zheng-rui~1; LI Xian-duan~

doi:10.13422/j.cnki.syfjx.2009.09.031

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Relativity between the Contents of Five Anthraquinones and the Appearance of Rhubarb Produced in Quanshui Village

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- Relativity between the Contents of Five Anthraquinones and the Appearance of Rhubarb Produced in Quanshui Village
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 15, Issue 9, Pages: 1-4(2009)
- 作者机构：
  
  1. 中国中医科学院中药研究所
  2. 甘肃神州红药材科技有限公司
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2009.09.031
  CLC： R284.1
- Published：2009
- 稿件说明：
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[1]代婉莹,孙维宏,毛淑杰,顾雪竹,钮正睿,李先端.铨水大黄外观性状与所含5种蒽醌成分含量的关系[J].中国实验方剂学杂志,2009,15(09):1-4.

DAI Wan-ying~1, SUN Wei-hong~2, MAO Shu-jie~1, et al. Relativity between the Contents of Five Anthraquinones and the Appearance of Rhubarb Produced in Quanshui Village[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(9): 1-4.
[1]代婉莹,孙维宏,毛淑杰,顾雪竹,钮正睿,李先端.铨水大黄外观性状与所含5种蒽醌成分含量的关系[J].中国实验方剂学杂志,2009,15(09):1-4. DOI： 10.13422/j.cnki.syfjx.2009.09.031.

DAI Wan-ying~1, SUN Wei-hong~2, MAO Shu-jie~1, et al. Relativity between the Contents of Five Anthraquinones and the Appearance of Rhubarb Produced in Quanshui Village[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(9): 1-4. DOI： 10.13422/j.cnki.syfjx.2009.09.031.

摘要

目的:研究铨水大黄中5种蒽醌成分分析方法

对经经验鉴别认为优、劣分成商品等级的铨水大黄进行成分分析

探讨成分含量与外观性状的相关性。方法:色谱柱填料为Kromasil-C18（4.6 mm×150 mm

5μm）

检测波长254 nm。流动相∶甲醇-0.1%磷酸溶液（85∶15）。结果:30%糠芯大黄与正常大黄比较

5种蒽醌成分含量下降约30%左右。同株大黄的无糠芯部位和糠芯部位相比

成分含量相差达70%

0%左右。浅黄色大黄5种蒽醌成分含量较黄色大黄含量也低

结论:该方法重复性好

测定结果表明成分含量与经验鉴别优、劣的大黄有一定的相关性。

Abstract

Objective:To develop the analytical method of five anthraquinones contained in rhubarb produced in Quanshui Village.To investigated the relativity between the contents of five constituents and the appearance.Method:The HPLC method is as follows:Kromasil-C

column（4.6 mm×150 mm

particle diameter 5 μm）

detective wavelength is 254 nm

methanol-0.1% phosphonic acid solution（85∶15） as mobile phase.Results:Compared with the high-grade rhubarb

the content of five anthraquinones in inferior ones descented about 30%.Compared with the high-grade part

the content of five constituents in the inferior part of the same root tuber descented about 70～80%.The contents of five anthraquinones in pale yellow rhubarb were lower than that in yellow ones.Conclusion: The method with fine repeatability is suitable to evaluate the contents of anthraquinones in rhubarb and the results indicate the contents of five constituents are associated with the appearance.

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Related Author

DAI Wan-ying1

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MAO Shu-jie1

GU Xue-zhu1

NIU Zheng-rui1

LI Xian-duan1

LI Wen-jing

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Related Institution

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Guangdong Provincial Enterprise Key Laboratory of Traditional Chinese Medicine Formula Granule，Guangdong Efong Pharmaceutical Co. Ltd.

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