Study on Primary Speciation of Mineral Elements in Ophicalcitum

FAN Li-bo; MENG Xian-sheng; ZHAO Jing; BAO Yong-rui; GUO Xiao-rui

doi:10.13422/j.cnki.syfjx.2010.14.028

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Study on Primary Speciation of Mineral Elements in Ophicalcitum

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- Study on Primary Speciation of Mineral Elements in Ophicalcitum
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 16, Issue 14, Pages: 35-37(2010)
- 作者机构：
  
  辽宁中医药大学药学院
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2010.14.028
  CLC： R284.1
- Published：2010
- 稿件说明：
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[1]范丽波,孟宪生,赵晶,包永睿,郭小瑞.花蕊石中9种无机元素初级形态研究[J].中国实验方剂学杂志,2010,16(14):35-37.

FAN Li-bo, MENG Xian-sheng, ZHAO Jing, et al. Study on Primary Speciation of Mineral Elements in Ophicalcitum[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(14): 35-37.
[1]范丽波,孟宪生,赵晶,包永睿,郭小瑞.花蕊石中9种无机元素初级形态研究[J].中国实验方剂学杂志,2010,16(14):35-37. DOI： 10.13422/j.cnki.syfjx.2010.14.028.

FAN Li-bo, MENG Xian-sheng, ZHAO Jing, et al. Study on Primary Speciation of Mineral Elements in Ophicalcitum[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(14): 35-37. DOI： 10.13422/j.cnki.syfjx.2010.14.028.

摘要

目的:测定中药花蕊石及水煎液中无机元素含量

对花蕊石无机元素的初级形态进行分析。方法:采用微波消解-电感耦合等离子体质谱法（ICP-MS）测定花蕊石中9种无机元素的含量

并进行了初级形态分析。结果:各元素在残渣中的含量均远远超过其在溶液中的含量。元素在原药中含量特征如下Mg>Ca>Fe>K>Zn>Mn>Cu

其中Se

K的提取率较高。结论:矿物药元素水煎液提取率和浸留比与植物药相比相对较小

花蕊石中Se

Cu可以认为是该药中作用最大的元素或最特征的元素。

Abstract

Objective:To determine the trace elements in traditional Chinese Medicine of ophicslcite and its decoction

and the primary speciation analysis on the trace elements of Ophicalcitum.Method:ICP-MS was used to determine the content of 13 trace elements and their primary speciation also been studied.Result:The content of elements in the residue was far more than the content in the solution.The content of elements in original drug was as follows:Mg > Ca > Fe > K > Zn > Mn > Cu

among which Se

K were in a higher extraction rate.Conclu-sion:The mineral medicine decoction extraction rate and the leaching residue ratio were relatively smaller than bo-tanical drug.In ophicslcite

Cu could be considered to be the two largest elements of the role of the drug or the most characteristic elements.

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Related Author

GUO Xiao-rui

BAO Yong-rui

FAN Li-bo

MENG Xian-sheng

ZHAO Jing

LI Juan

ZHENG Guohua

CAO Yan

Related Institution

School of Pharmacy，Hubei University of Chinese Medicine

Institute of Chinese Meteria Medica,China Academy of Chinese Medical Sciences

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