WEI Jian-hua, CAI Shao-fang, ZHEN Han-shen, et al. Chemical Constituents form Exocarp of Diospyros kaki[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(14): 102-104.
WEI Jian-hua, CAI Shao-fang, ZHEN Han-shen, et al. Chemical Constituents form Exocarp of Diospyros kaki[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(14): 102-104. DOI: 10.13422/j.cnki.syfjx.2010.14.050.
Chemical Constituents form Exocarp of Diospyros kaki
摘要
目的:研究柿皮Diospyros kaki的化学成分。方法:采用硅胶柱色谱方法分离纯化
通过1H-NMR
13C-NMR
MS
IR等波谱方法以及化合物的理化性质进行结构鉴定。结果:从柿皮中分离得到7个化合物
分别鉴定为棕榈酸(1)
β-谷甾醇(2)
乌苏酸(3)
24-丙基-3β-羟基-胆甾-5-烯(4)
齐墩果酸(5)
东莨菪内酯(6)
肉豆蔻酸(7)。结论:化合物4
6
7均首次从该植物中分离得到。
Abstract
Objective:To study the chemical constituents from exocaep of Diospyros kaki.Method:Compounds were isolated by chromatographic techniques.The structures were identified by physicochemical properties and spectral analyses(1H-NMR
13 C-NMR
MS and IR).Result:Seven compounds were isolated and identified as palmitic acid(1)
β-sitosterol(2)
ursolic acid(3)
24R-24-propylcholest-5-en-3β-ol(4)
oleanolic acid(5)
scopoletin(6)
myristic acid(7).Conclusion:Compounds 4
6
7 were obtained from this plant for the first time.
In Vitro and in vivo Component Identification of DanshenyinBased on UPLC-Q-TOF-MS/MS
Identification of in Vitro and in vivo Chemical Constituents of Ruyi Zhenbaowan Based on UHPLC-Q Exactive Orbitrap HRMS
Progress in Research on Effect of Processing on Chemical Constituents and Pharmacological Effect of Notoginseng Radix et Rhizoma
Correlation Between Chemical Constituents and Ecological Factors of Tibetan Medicine Swertia mussotii
Related Author
WEI Jian-hua
CAI Shao-fang
ZHEN Han-shen
MO Qiu-mei
ZHANG Sitong
HU Xianrun
LIU Wenkang
LEI Jinchun
Related Institution
Key Laboratory for Standardization of Chinese Medicines,Ministry of Education, Shanghai Key Laboratory for Compound Chinese Medicines,Institute of Chinese Materia Medica, Shanghai University of Traditional Chinese Medicine
Arura Tibetan Medicine Co.Ltd.
Institute of Chinese Materia Medica,China Academy of Chinese Medical Sciences
School of TCM,Guangdong Pharmaceutical University
Key Laboratory of Basic and Applied Research of Northern Medicine,Ministry of Education,Heilongjiang Key Laboratory of Pharmacodynamic Material Basis of Traditional Chinese Medicine (TCM) and Natural Medicine,Heilongjiang University of Chinese Medicine