Comparison of Total Cantharidin Contents in Blister Beetle before and after Processed by HPLC

ZHAO Li-na1; SHI Yan-bang1; ZHANG Zhen-ling1; ZHANG Ben-shan1

doi:10.13422/j.cnki.syfjx.2010.15.021

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Comparison of Total Cantharidin Contents in Blister Beetle before and after Processed by HPLC

更新时间：2024-09-23

- Comparison of Total Cantharidin Contents in Blister Beetle before and after Processed by HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 16, Issue 15, Pages: 39-41(2010)
- 作者机构：
  
  1. 河南中医学院
  2. 郑州铁路职业技术学院
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2010.15.021
  CLC： R284.1
- Published：2010
- 稿件说明：
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[1]赵丽娜,石延榜,张振凌,张本山.中药斑蝥不同炮制品总斑蝥素含量的比较[J].中国实验方剂学杂志,2010,16(15):39-41.

ZHAO Li-na1, SHI Yan-bang1, ZHANG Zhen-ling1, et al. Comparison of Total Cantharidin Contents in Blister Beetle before and after Processed by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(15): 39-41.
[1]赵丽娜,石延榜,张振凌,张本山.中药斑蝥不同炮制品总斑蝥素含量的比较[J].中国实验方剂学杂志,2010,16(15):39-41. DOI： 10.13422/j.cnki.syfjx.2010.15.021.

ZHAO Li-na1, SHI Yan-bang1, ZHANG Zhen-ling1, et al. Comparison of Total Cantharidin Contents in Blister Beetle before and after Processed by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(15): 39-41. DOI： 10.13422/j.cnki.syfjx.2010.15.021.

摘要

目的:建立测定不同斑蝥炮制品及斑蝥虫体各部位中总斑蝥素的含量的方法

探讨炮制对总斑蝥素的影响。方法:HPLC

以甲醇-水（23∶77）为流动相

柱温35℃

流速为1 mL.min-1

检测波长为230 nm。结果:斑蝥总斑蝥素含量远高于药典规定。样品中总斑蝥素含量:生斑蝥饮片>斑蝥药材>米炒斑蝥。头足翅中总斑蝥素的总含量为0.61%。结论:应以总斑蝥素含量控制斑蝥饮片质量。

Abstract

Objective:The contents in different samples and different parts of the beetle were determined to study the impact of processing blister beetle on the total cantharidin contents.Method:HPLC conditions were as follows:the mobile phase was methanol-water（23∶77）;the column temperature was at 35℃;the flow rate was 1.0 mL.min-1;the detection wavelength was at 230 nm.Result: The total cantharidin contents determined were: unprocessed mylabris>blister beetle>mylabris（stir-frying with rice）.The total contents of head

legs

inside and outside wings of blister beetle were 0.61%.Conclusion:For safety

the total cantharidin contents should be used to control the quality of blister beetle.

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Related Author

ZHAO Li-na

SHI Yan-bang

ZHANG Zhen-ling

ZHANG Ben-shan

Hong-xing MA

Long-fei LIN

Yu-ling LIU

Sai FU

Related Institution

Jilin Agricultural University

Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences

Chengde Medical University

Jilin Huakang Pharmaceutical Co. Ltd.

The First Clinical Medical College of Guangzhou University of Chinese Medicine

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