Determination of Ginsenoside Rg<sub>1</sub> and Notoginsenoside R<sub>1</sub> in Yirenchangtai Capsules by HPLC

WANG Fang 1; LI Xue-qing2; ZHANG Xing1; MA Tong3; YU Lei3; LIU Zi-dong1; LIU Yu-lin1

doi:10.13422/j.cnki.syfjx.2010.15.032

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Determination of Ginsenoside Rg₁ and Notoginsenoside R₁ in Yirenchangtai Capsules by HPLC

更新时间：2024-09-23

- Determination of Ginsenoside Rg₁ and Notoginsenoside R₁ in Yirenchangtai Capsules by HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 16, Issue 15, Pages: 72-74(2010)
- 作者机构：
  
  1. 第四军医大学基础部药品研发中心
  2. 第四军医大学西京医院药剂科
  3. 西安交通大学第一附属医院药剂科
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2010.15.032
  CLC： R286
- Published：2010
- 稿件说明：
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[1]王芳,李雪晴,张星,马侗,余蕾,刘子冬,刘玉林.HPLC同时测定薏仁肠肽胶囊中人参皂苷Rg_1和三七皂苷R_1含量[J].中国实验方剂学杂志,2010,16(15):72-74.

WANG Fang 1, LI Xue-qing2, ZHANG Xing1, et al. Determination of Ginsenoside Rg₁ and Notoginsenoside R₁ in Yirenchangtai Capsules by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(15): 72-74.
[1]王芳,李雪晴,张星,马侗,余蕾,刘子冬,刘玉林.HPLC同时测定薏仁肠肽胶囊中人参皂苷Rg_1和三七皂苷R_1含量[J].中国实验方剂学杂志,2010,16(15):72-74. DOI： 10.13422/j.cnki.syfjx.2010.15.032.

WANG Fang 1, LI Xue-qing2, ZHANG Xing1, et al. Determination of Ginsenoside Rg₁ and Notoginsenoside R₁ in Yirenchangtai Capsules by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(15): 72-74. DOI： 10.13422/j.cnki.syfjx.2010.15.032.

摘要

目的:采用反相高效液相色谱法测定薏仁肠肽胶囊中人参皂苷Rg1和三七皂苷R1含量。方法:采用色谱柱为Agilent ZE-C18柱（4.6 mm×250 mm

5μm）

以乙腈-水（17∶83）为流动相

流速为1.0 mL.min-1

检测波长为203 nm。结果:人参皂苷Rg1在0.4～10.1μg呈良好的线性关系

r=0.999 8

三七皂苷R1在0.1～2.5μg呈良好的线性关系

r=0.999 8

人参皂苷Rg1平均回收率99.96%

RSD为0.25%

三七皂苷R1平均回收率100.03%

RSD为0.23%。结论:本法可同时测定薏仁肠肽胶囊中人参皂苷Rg1和三七皂苷R1含量

方法可靠、准确。

Abstract

Objective:To determine Determination ginsenoside Rg1 and notoginsenoside R1in Yirenchangtai Capsules by HPLC.Method:The separation was performed on Agilent ZE-C18 column

using methyl cyanide-water（17∶83）as mobile phase.The detection wavelength was at 203 nm.The flow rate was 1.0 mL·min-1.Result:The linear range of ginsenoside Rg1 was 0.4-10.1 μg（r=0.999 6）

The linear range of notoginsenoside R1 was 0.1-0.25 μg（r=0.999 6）.The average recovery of ginsenoside Rg1 was 99.96%

RSD was 0.25%（n=6）.The average recovery of notoginsenoside R1 was 100.03%

RSD was 0.23%（n=6）.Conclusion: The method can determine the ginsenoside Rg1and notoginsenoside R1 The method was reliable and accura.

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Related Author

WANG Fang

LI Xue-qing

ZHANG Xing

MA Tong

YU Lei

LIU Zi-dong

LIU Yu-lin

LIU En-li

Related Institution

Guangdong Institute of Traditional Chinese Medicine

School of Pharmaceutical Science,Shanxi Medical University

Shanxi Province Chinese Medicine Modern Engineering Technology Research Center

Guangzhou University of Chinese Medicine

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Determination of Ginsenoside Rg1 and Notoginsenoside R1 in Yirenchangtai Capsules by HPLC

DOI：10.13422/j.cnki.syfjx.2010.15.032

摘要

Abstract

关键词

Keywords

references

Determination of Ginsenoside Rg₁ and Notoginsenoside R₁ in Yirenchangtai Capsules by HPLC