Study on Quality Standard of Antiasthmatic Dropping Pills

ZHOU Bin1; LI Yan-xia2; ZHU Cai-qing2; CHANG Jun1; WEI Dong-zhi3

doi:10.13422/j.cnki.syfjx.2011.01.025

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Study on Quality Standard of Antiasthmatic Dropping Pills

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- Study on Quality Standard of Antiasthmatic Dropping Pills
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 1, Pages: 43-45(2011)
- 作者机构：
  
  1. 江西科技师范学院药学院
  2. 江西省药物研究所
  3. 华东理工大学生物反应器工程国家重点实验室
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2011.01.025
  CLC： R286
- Published：2011
- 稿件说明：
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[1]周斌,李雁霞,朱才庆,常军,魏东芝.抗平喘滴丸质量标准研究[J].中国实验方剂学杂志,2011,17(01):43-45.

ZHOU Bin1, LI Yan-xia2, ZHU Cai-qing2, et al. Study on Quality Standard of Antiasthmatic Dropping Pills[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(1): 43-45.
[1]周斌,李雁霞,朱才庆,常军,魏东芝.抗平喘滴丸质量标准研究[J].中国实验方剂学杂志,2011,17(01):43-45. DOI： 10.13422/j.cnki.syfjx.2011.01.025.

ZHOU Bin1, LI Yan-xia2, ZHU Cai-qing2, et al. Study on Quality Standard of Antiasthmatic Dropping Pills[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(1): 43-45. DOI： 10.13422/j.cnki.syfjx.2011.01.025.

摘要

目的:建立一种抗平喘滴丸的质量标准。方法:采用薄层色谱（TLC）对处方中药材进行鉴别

采用高效液相色谱（HPLC）测定滴丸中麻黄碱和伪麻黄碱的含量。结果:TLC图谱中可检出苦杏仁、甘草、麻黄的特征图谱

盐酸麻黄碱进样量在0.033 05～0.396 6μg线性关系良好

r=0.999 9

平均回收率99.39%

RSD 2.11%（n=6）。盐酸伪麻黄碱进样量在0.023～0.276μg线性关系良好。r=0.999 7

平均回收率99.89%

RSD 2.55%（n=6）。结论:所建方法简单准确

重复性好

可用于本品的质量控制。

Abstract

Objective:To set up the quality standard of antiasthmatic dropping pills.Method: TLC was used for identification;ephedrine hydrochloride and pseudoephedrine hydrochloride were determined by HPLC.Result: Prunus armeniaca L.var.ansu Maxim.

Glycyrrhiza uralensis Fisch.and Ephedra sinica Stapf.could be detected by TLC.Ephedrine hydrochloride was linear in the range of 0.033 05-0.396 6 μg（r = 0.999 9）;the average recovery was 99.39%（RSD 2.11%

n = 6）.Pseudoephedrine hydrochloride was linear in the range of 0.023-0.276 μg（r = 0.999 7）;the average recovery was 99.89%（RSD 2.55%

n = 6）.Conclusion: The method was simple and accu-rate with a good reproducibility

and can be used for the quality control of antiasthmatic dropping pills.

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