Identification and Determination of Paeonol of Rukang Tincture

LIU Zhi-sheng1; LI Jia1; HUANG Jian-you1; HUANG Rui-song2

doi:10.13422/j.cnki.syfjx.2011.02.021

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Identification and Determination of Paeonol of Rukang Tincture

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- Identification and Determination of Paeonol of Rukang Tincture
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 2, Pages: 50-52(2011)
- 作者机构：
  
  1. 广西中医药研究院
  2. 广西民族医药研究所
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2011.02.021
  CLC： R286
- Published：2011
- 稿件说明：
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[1]刘智生,李嘉,黄建猷,黄瑞松.乳康酊的薄层鉴别及丹皮酚的含量测定[J].中国实验方剂学杂志,2011,17(02):50-52.

LIU Zhi-sheng1, LI Jia1, HUANG Jian-you1, et al. Identification and Determination of Paeonol of Rukang Tincture[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(2): 50-52.
[1]刘智生,李嘉,黄建猷,黄瑞松.乳康酊的薄层鉴别及丹皮酚的含量测定[J].中国实验方剂学杂志,2011,17(02):50-52. DOI： 10.13422/j.cnki.syfjx.2011.02.021.

LIU Zhi-sheng1, LI Jia1, HUANG Jian-you1, et al. Identification and Determination of Paeonol of Rukang Tincture[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(2): 50-52. DOI： 10.13422/j.cnki.syfjx.2011.02.021.

摘要

目的:建立乳康酊薄层鉴别和含量测定的方法。方法:采用薄层色谱法对乳康酊中徐长卿、龙血竭进行定性鉴别;采用高效液相色谱法测定制剂中丹皮酚的含量。结果:在薄层色谱中可检出徐长卿和龙血竭;丹皮酚在0.03～0.27 g.L-1与峰面积呈良好的线性关系（r=0.999 9）

平均加样回收率为99.01%

RSD 2.22%（n=6）。结论:所建立的方法简便、准确、可靠

可用于该制剂的质量控制。

Abstract

Objective:To establish an identification and conten determination methods of Rukang Tincture.Method:Radix Cynanchi Paniculati and Resina Draconis were identified by TLC.The content of paeonol in Rukang tincture was determined by HPLC.Result:Radix Cynanchi Paniculati and Resina Draconis could be detected by TLC.Determine the content of paeonol by HPLC

paeonol showed a good linear relationship at a range of 0.03-0.27 g·L-1（r = 0.999 9）.The average recovery rate was 99.01% with RSD of 2.22%（n = 6）.Conclusion:The established methods are simple

accurate

reliable and can be used for the quality control of Rukang tincture.

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Related Author

LIU Zhi-sheng

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LIU Zhi-sheng1

HUANG Rui-song2

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Related Institution

Taiyuan Institute for Food and Drug Control,Taiyan

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