HPLC Fingerprint of Hemostatic Fraction of Rehmannia glutinosa

GUO Dong-yan1; ZHANG Li-juan1; WANG Mei2; SHI Yan-qiong1

doi:10.13422/j.cnki.syfjx.2011.04.033

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HPLC Fingerprint of Hemostatic Fraction of Rehmannia glutinosa

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- HPLC Fingerprint of Hemostatic Fraction of Rehmannia glutinosa
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 4, Pages: 90-92(2011)
- 作者机构：
  
  1. 陕西中医学院
  2. 陕西中医学院附属医院制剂中心
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2011.04.033
  CLC： R284.1
- Published：2011
- 稿件说明：
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[1]郭东艳,张丽娟,王梅,师延琼.生地黄止血有效部位HPLC指纹图谱研究[J].中国实验方剂学杂志,2011,17(04):90-92.

GUO Dong-yan1, ZHANG Li-juan1, WANG Mei2, et al. HPLC Fingerprint of Hemostatic Fraction of Rehmannia glutinosa[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(4): 90-92.
[1]郭东艳,张丽娟,王梅,师延琼.生地黄止血有效部位HPLC指纹图谱研究[J].中国实验方剂学杂志,2011,17(04):90-92. DOI： 10.13422/j.cnki.syfjx.2011.04.033.

GUO Dong-yan1, ZHANG Li-juan1, WANG Mei2, et al. HPLC Fingerprint of Hemostatic Fraction of Rehmannia glutinosa[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(4): 90-92. DOI： 10.13422/j.cnki.syfjx.2011.04.033.

摘要

目的:研究生地黄止血有效部位HPLC指纹图谱。方法:采用高效液相色谱法

Akasil-C18柱（4.6 mm×250 mm

5μm）

乙腈-水梯度洗脱

检测波长210 nm

流速1.0 mL.min-1

柱温30℃。结果:确定了生地黄止血有效部位的10批指纹图谱共有模式

进行了相似度比较。结论:所建立的方法可用于生地黄止血有效部位指纹图谱测定

并可对其制剂的质量评价提供科学依据。

Abstract

Objective:HPLC fingerprints of the hemostatic fraction of Rehmannia glutinosa were estab-lished.Method: Akasil C18（4.6 mm × 250 mm

5 μm） column was used and the acetonitrile-water was chosen as the mobile phase in a gradient mode.The column temperature was at 30 ℃ and the detection wavelength was at 210 nm.The detection time was 60 min

and the flow rate was 1.0 mL.min-1.Result:Fifteen characteristic peaks were indicated in HPLC fingerprints.The relative retention time is as of the common peaks were also determined.Conclu-sion: The method established is simple and accurate with a good reproducibility and will provide a reference stand-ard for the quality control of R.glutinosa.

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Related Author

GUO Dong-yan

ZHANG Li-juan

WANG Mei

SHI Yan-qiong

HOU Mengyu

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Related Institution

Nanchang Medical College

Jiangxi University of Chinese Medicine

Jiangxi Jingde Traditional Chinese Medicine Co. Ltd.

School of Pharmacy， Jiangxi University of Chinese Medicine

Institute of Chinese Materia Medica，China Academy of Chinese Medical Sciences

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