Study on Extraction Technology of Synephrine in Citrus aurantium by Orthogonal Design

LIAO Mao-liang1; HU Jing2; SHANG Hai-hua1; WANG Yang2; ZHANG Tie-jun1

doi:10.13422/j.cnki.syfjx.2011.13.025

您当前的位置：

首页 >

文章列表页 >

Study on Extraction Technology of Synephrine in Citrus aurantium by Orthogonal Design

更新时间：2024-09-23

- Study on Extraction Technology of Synephrine in Citrus aurantium by Orthogonal Design
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 13, Pages: 23-25(2011)
- 作者机构：
  
  1. 天津药物研究院
  2. 天津中医药大学
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2011.13.025
  CLC： R284
- Published：2011
- 稿件说明：
移动端阅览
[1]廖茂梁,胡静,尚海花,王阳,张铁军.正交试验优选枳实中辛弗林提取工艺[J].中国实验方剂学杂志,2011,17(13):23-25.

LIAO Mao-liang1, HU Jing2, SHANG Hai-hua1, et al. Study on Extraction Technology of Synephrine in Citrus aurantium by Orthogonal Design[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(13): 23-25.
[1]廖茂梁,胡静,尚海花,王阳,张铁军.正交试验优选枳实中辛弗林提取工艺[J].中国实验方剂学杂志,2011,17(13):23-25. DOI： 10.13422/j.cnki.syfjx.2011.13.025.

LIAO Mao-liang1, HU Jing2, SHANG Hai-hua1, et al. Study on Extraction Technology of Synephrine in Citrus aurantium by Orthogonal Design[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(13): 23-25. DOI： 10.13422/j.cnki.syfjx.2011.13.025.

摘要

目的:研究枳实中辛弗林的最佳提取工艺。方法:以辛弗林的转移率为指标

考察了不同提取溶剂和提取方式对辛弗林提取率的影响

在此基础上采用正交试验设计

考察了加水量、煎煮温度、煎煮时间3个因素对辛弗林提取率的影响。结果:加水回流提取辛弗林的提取率较高

确定枳实的最佳提取工艺为:回流提取3次

提取1 h

加水依次为12

10倍量。结论:工艺条件简单

稳定

可行

辛弗林提取率高

为改进枳实的提取工艺提供了依据。

Abstract

Objective:To optimize the extraction process for synephrine in Citrus aurantium.Method: According to the yield rate of synephrine

the use of extraction solvent and distilling methods was studied.And L9（34） orthogonal design was used to determine the optimum extraction conditions.Three factors were studied as indexes that might affect the yield rate of synephrine

including water quantity

extraction temperature and time required.Result: The yield rate of synephrine in the water extraction was obviously higher than that in the other distilling methods.The optimized extraction procedure was as follows: refluxed three times

1.0 hour each time

the amount of water was 12

10 in turn.Conclusion: This extraction method is convenient and feasible

and can improve the extraction of synephrine from Citrus aurantium.

关键词

Keywords

references

Views

630

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Quality Control of Standard Decoction of Aurantii Fructus Immaturus

Study on the Extraction Process for Total Glucosides of Yupingfeng with Orthogonal Design

Study on the Technology of Extraction and Purification of Flavonoies from Herba Potentillae Chinensis

Progress in the Study on Extraction and Purification of Diterpenes Compounds

Related Author

LIAO Mao-liang

HU Jing

SHANG Hai-hua

WANG Yang

ZHANG Tie-jun

Jia SHI

Wen-guang JING

Zhe DENG

Related Institution

Institute of Traditional Chinese Medicine(TCM), China National TCM Co. Ltd.

Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences

Dongguan Hospital of Traditional Chinese Medicine

Affiliated Hospital of Guilin Medical College

Guilin Medical University

AI问答

Postal code：100700
Tel：010-84076882 Email：syfjx_2010@188.com
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备11006657号-10 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰