Determination of Naringin,Hesperidin and Baicalin in Tongxuan Lifei Capsules

TANG De-zhi

doi:10.13422/j.cnki.syfjx.2011.15.002

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Determination of Naringin,Hesperidin and Baicalin in Tongxuan Lifei Capsules

更新时间：2024-09-23

- Determination of Naringin,Hesperidin and Baicalin in Tongxuan Lifei Capsules
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 15, Pages: 93-95(2011)
- 作者机构：
  
  广西南宁食品药品检验所
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2011.15.002
  CLC： TQ461
- Published：2011
- 稿件说明：
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[1]唐德智.通宣理肺胶囊中柚皮苷、橙皮苷和黄芩苷的含量测定[J].中国实验方剂学杂志,2011,17(15):93-95.

TANG De-zhi. Determination of Naringin,Hesperidin and Baicalin in Tongxuan Lifei Capsules[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(15): 93-95.
[1]唐德智.通宣理肺胶囊中柚皮苷、橙皮苷和黄芩苷的含量测定[J].中国实验方剂学杂志,2011,17(15):93-95. DOI： 10.13422/j.cnki.syfjx.2011.15.002.

TANG De-zhi. Determination of Naringin,Hesperidin and Baicalin in Tongxuan Lifei Capsules[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(15): 93-95. DOI： 10.13422/j.cnki.syfjx.2011.15.002.

摘要

目的:建立HPLC同时测定通宣理肺胶囊中柚皮苷、橙皮苷、黄芩苷的含量。方法:色谱柱Agilent ZORBAX SB-C18（4.6 mm×250 mm

5μm）;流动相乙腈-0.1%磷酸溶液（21∶79）

检测波长280 nm

流速1.0 mL.min-1

柱温30℃。结果:柚皮苷进样量在0.156～1.408μg线性关系良好（r=0.999 8

n=5）

平均回收率99.56%

RSD 0.88%（n=9）;橙皮苷进样量在0.145～1.301μg线性关系良好（r=0.999 7

n=5）

平均回收率99.83%

RSD 0.66%（n=9）。黄芩苷进样量在0.359～3.233μg线性关系良好（r=0.999 9

n=5）

平均回收率为98.94%

RSD 1.55%（n=9）;结论:该方法操作简便

准确可靠

可作为通宣理肺胶囊的质量控制。

Abstract

Objective:To establish an HPLC method for determination of naringin

hesperidin and baicalin in Tongxuan Lifei capsules. Method:The chromatographic column of Agilent ZORBAX SB C18（ 4. 6 mm × 250 mm

5 μm） was used

the mobile phase was consisted of acetonitrile-0. 1% phosphoric acid aqueous solution（ 21:79） .The flow rate was 1. 0 mL· min -1

the detective wavelength was 280 nm and column temperature was 30 ℃ .Result: The linear range of naringin

hesperidin and Baicalin were 0. 156-1. 408 μg（ r=0. 999 8）

0. 145-1. 301 μg（ r=0. 999 7） and 0. 359-3. 233 μg（ r=0. 999 9）

the average recoveries （n=9） were 99. 56% （ RSD 0. 88% ）

were 99. 83% （ RSD 0. 66% ） and 98. 94% （ RSD 1. 55% ） respectively. Conclusion: The results showed thismethod is accurate

reproducible

simple and easy to do

which can be used in quality control of Tongxuan Lifei Capsules.

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