Extracting Technology For Gushu Capsule

XIE Shan1; JIA Xian-sheng2

doi:10.13422/j.cnki.syfjx.2011.15.026

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Extracting Technology For Gushu Capsule

更新时间：2024-09-23

- Extracting Technology For Gushu Capsule
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 15, Pages: 49-52(2011)
- 作者机构：
  
  1. 贵阳中医学院第二附属医院
  2. 贵阳中医学院
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2011.15.026
  CLC： R286
- Published：2011
- 稿件说明：
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[1]谢珊,贾宪生.骨舒胶囊的提取工艺优选[J].中国实验方剂学杂志,2011,17(15):49-52.

XIE Shan1, JIA Xian-sheng2. Extracting Technology For Gushu Capsule[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(15): 49-52.
[1]谢珊,贾宪生.骨舒胶囊的提取工艺优选[J].中国实验方剂学杂志,2011,17(15):49-52. DOI： 10.13422/j.cnki.syfjx.2011.15.026.

XIE Shan1, JIA Xian-sheng2. Extracting Technology For Gushu Capsule[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(15): 49-52. DOI： 10.13422/j.cnki.syfjx.2011.15.026.

摘要

目的:优选骨舒胶囊的提取工艺。方法:采用正交试验方法对影响水提取醇沉工艺的各因素进行考察

以HPLC测定淫羊藿苷的含量作为优选工艺的考察指标。结果:优选的最佳工艺为药材加10倍量水

煎煮1 h

煎煮3次;醇沉时浸膏相对密度为1.08（60℃）

药液温度为40℃

加醇至60%。结论:按正交试验优选的提取工艺可行

以淫羊藿苷为指标成分

能较好控制提取工艺的质量

方法简便实用。

Abstract

Objective:To optimize the extraction technology of Gushu capsules.Method:The optimal technology was obtained by orthogonal design test.The icatiin in decoction liquid and ethanol precipitation liquid was determined by HPLC as examination target.Result:The optimal extraction technology of Gushu capsules was as follows:decoction liquid method with 10 times volume of water

extracted 3 times and for 1 h at each time.The ethanol precipitation method with temperature is at 40 ℃

adding ethanol to 60%

laying 3 days.Conclusion:The extraction technology is rational and feasible.The method is practical and can easily control the extpaction rechnology with icariin as terget ingredient.

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LIU Qi-hua

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CHEN Hong-gang

Related Institution

Graduate School，Beijing University of Chinese Medicine

The First Affiliated Hospital，Baotou Medical College，Inner Mongolia University of Science and Technology

Peking University Health Science Center

Japan Friendship Hospital

Guizhou University of Traditional Chinese Medicine（TCM）

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