Studies on Quality Standard of Xingshen Spray

KE Xue-hong; MENG Zhi-kang; MO Zhen-tao; ZHANG Jin; FANG Yong-qi

doi:10.13422/j.cnki.syfjx.2011.15.034

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Studies on Quality Standard of Xingshen Spray

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- Studies on Quality Standard of Xingshen Spray
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 15, Pages: 76-79(2011)
- 作者机构：
  
  广州中医药大学第一附属医院实验中心
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2011.15.034
  CLC： R286.0
- Published：2011
- 稿件说明：
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[1]柯雪红,蒙治康,莫镇涛,张瑾,方永奇.醒神喷鼻液质量标准研究[J].中国实验方剂学杂志,2011,17(15):76-79.

KE Xue-hong, MENG Zhi-kang, MO Zhen-tao, et al. Studies on Quality Standard of Xingshen Spray[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(15): 76-79.
[1]柯雪红,蒙治康,莫镇涛,张瑾,方永奇.醒神喷鼻液质量标准研究[J].中国实验方剂学杂志,2011,17(15):76-79. DOI： 10.13422/j.cnki.syfjx.2011.15.034.

KE Xue-hong, MENG Zhi-kang, MO Zhen-tao, et al. Studies on Quality Standard of Xingshen Spray[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(15): 76-79. DOI： 10.13422/j.cnki.syfjx.2011.15.034.

摘要

目的:建立醒神喷鼻液的质量标准。方法:采用TLC鉴别方中石菖蒲挥发油、冰片及猪牙皂。用HPLC测定β-细辛醚、麝香酮的含量。结果:TLC色谱中分别检出石菖蒲挥发油、β-细辛醚、冰片及猪牙皂

阴性对照无干扰。β-细辛醚、麝香酮分别在0.174 4～0.872 0μg（r=0.999 8）、0.214～1.07μg（r=0.9994）呈良好的线性关系

平均加样回收率分别为99.96%（RSD 2.61%

n=6）

100.17%（RSD 3.36%

n=6）。结论:研究建立的TLC和HPLC方法专属性强、灵敏度高、重现性好

可用于醒神喷鼻液的质量控制。

Abstract

Objective:To establish the quality standard of Xingshen spray.Method:TLC was used too distinguish Volatile oil of Rhizoma Acori Tatarinowii

Borneolum Syntheticum and fructus Gleditsiae abnormalis.HPLC was used for the determination of β-asarone and Muscone.Result:The thin-layer chromatography spots were clear and the negative samples had no interferences

β-asarone and Muscone were linear in the range of 0.174 4-0.872 0 μg（r=0.999 8）

0.214-1.07 μg（r=0.999 4）

and the average recovery was 99.96%（RSD 2.61%

n=6）

100.17%（RSD 3.36%

n=6）.Conclusion:This method is simple

accurate

reliable and can be used as a quality control method for Xingshen spray.

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Related Author

KE Xue-hong

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FANG Yong-qi

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HUANG Rui-song2

Related Institution

Taiyuan Institute for Food and Drug Control,Taiyan

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