GC-MS Analysis of Huoluo Oil

ZHAO Xin1; ZHU Ling2; XIAO Yu-ping1; HUANG Bi-yun3

doi:10.13422/j.cnki.syfjx.2011.15.047

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GC-MS Analysis of Huoluo Oil

更新时间：2024-09-23

- GC-MS Analysis of Huoluo Oil
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 15, Pages: 116-118(2011)
- 作者机构：
  
  1. 广东轻工职业技术学院食品与生物工程系
  2. 江苏正大天晴药业股份有限公司
  3. 广州医学院药物研究中心
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2011.15.047
  CLC： R284.1
- Published：2011
- 稿件说明：
移动端阅览
[1]赵鑫,朱玲,肖玉平,黄碧云.活络油化学成分的GC-MS分析[J].中国实验方剂学杂志,2011,17(15):116-118.

ZHAO Xin1, ZHU Ling2, XIAO Yu-ping1, et al. GC-MS Analysis of Huoluo Oil[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(15): 116-118.
[1]赵鑫,朱玲,肖玉平,黄碧云.活络油化学成分的GC-MS分析[J].中国实验方剂学杂志,2011,17(15):116-118. DOI： 10.13422/j.cnki.syfjx.2011.15.047.

ZHAO Xin1, ZHU Ling2, XIAO Yu-ping1, et al. GC-MS Analysis of Huoluo Oil[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(15): 116-118. DOI： 10.13422/j.cnki.syfjx.2011.15.047.

摘要

目的:对活络油中的化学成分进行气相色谱-质谱（GC-MS）分析。方法:采用HP-5ms UI石英毛细管柱

程序升温

以EI离子源和四级杆质量分析器对试样进行分析

质谱图采用NIST 2008谱库检索

结合人工谱图分析

鉴定主要化学成分

并用归一化法测定其相对含量。结果:试样分离出33个色谱峰

共鉴定了其中30个化合物

占总峰面积的99%以上

活络油主要成分为α-蒎烯（8.41%）、桉油精（5.59%）、右旋樟脑（11.7%）、右旋薄荷脑（31.31%）、水杨酸甲酯（25.69%）、茴香脑（2.83%）、丁香酚（4.24%）等。结论:活络油化学成分主要为萜类化合物、芳香族化合物和脂肪族化合物等。

Abstract

Objective:To develop a GC-MS method to analyze the chemical composition of Huoluo oil.Method:A capillary column HP-5ms UI was used.The column temperature was controlled by a program and the MS analysis was performed with EI and quadrupolemass analyzer.The chemical composition was identified by NIST 2008 searching and mass spectra comparing and their relative contents were calculated by area normalization method.Result:Thirty-three peaks were separated and 30 compounds have been identified

which accounted for over 99% of the peak areas of essential oil.The major components of Huoluo oil were alpha-pinene（8.41%）

eucalyptol（5.59%）

D-camphor（11.7%）

D-menthol（31.31%）

methyl salicylate（25.69%）

anethole（2.83%

）

eugenol（4.24%）

et al.Conclusion:The present study provide scientific bases for exploitation of Huoluo oil.

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Related Author

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Related Institution

Shenzhen Municipal Institute for Drug Control

深圳市药品检验所广东深圳518029

Guangxi college of Traditional Chinese Medical

Institute of Chinese Materia Medica，China Academy of Chinese Medical Sciences

Gansu Taikang Pharmaceutical Co. Ltd.

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