Determination of Mangiferin in Anshenjiaonang by HPLC

XU Meng-wen1; CHEN Tong-kai1; AN Hui-wei1; XIE Zhu-tian1; HE Min-xia2

doi:10.13422/j.cnki.syfjx.2011.23.055

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Determination of Mangiferin in Anshenjiaonang by HPLC

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- Determination of Mangiferin in Anshenjiaonang by HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 23, Pages: 77-78(2011)
- 作者机构：
  
  1. 广州医药工业研究院
  2. 广东药学院
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2011.23.055
  CLC： R286
- Published：2011
- 稿件说明：
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[1]徐孟文,陈桐楷,安穗伟,谢柱添,何敏霞.HPLC测定安神胶囊中芒果苷含量[J].中国实验方剂学杂志,2011,17(23):77-78.

XU Meng-wen1, CHEN Tong-kai1, AN Hui-wei1, et al. Determination of Mangiferin in Anshenjiaonang by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(23): 77-78.
[1]徐孟文,陈桐楷,安穗伟,谢柱添,何敏霞.HPLC测定安神胶囊中芒果苷含量[J].中国实验方剂学杂志,2011,17(23):77-78. DOI： 10.13422/j.cnki.syfjx.2011.23.055.

XU Meng-wen1, CHEN Tong-kai1, AN Hui-wei1, et al. Determination of Mangiferin in Anshenjiaonang by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(23): 77-78. DOI： 10.13422/j.cnki.syfjx.2011.23.055.

摘要

目的:建立HPLC测定安神胶囊中芒果苷的含量测定方法。方法:采用HPLC测定芒果苷的含量

Diamonsil C18（4.6 mm×250 mm

5μm）为色谱柱

流动相乙腈-0.2%冰醋酸水溶液（15∶85）

流速1 mL.min-1

检测波长258 nm

进样量10μL。结果:芒果苷在2.5～7.5 mg.L-1呈良好的线性关系（r=0.999 8）

回收率99.58%（RSD 0.79%

n=9）。结论:方法简便

准确

灵敏度高

重复性好

可用于安神胶囊中知母有效成分芒果苷的含量测定。

Abstract

Objective:To establish a quantitative method for detarminazion of mangiferin in Anshen capsule by HPLC.Method: Using a HPLC method was used with Diamonsil C18（4.6 mm×250 mm

5 μm）

the mobile phase was acetonitrile-0.2% phosphate（15∶85） at a flow rate of 1 mL·min-1

the UV detection wavelength was 258 nm.Result: The linear range of mangiferin was in the range between 2.5 mg·L-1 and 7.5 mg·L-1（r=0.999 8）.The average recovery of mangiferin was 99.58% with RSD of 0.79%.Conclusion: This method is simple

efficient and accurate

which can be used for the quality control of mangiferin in Anshen capsule.

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Related Author

XU Meng-wen

CHEN Tong-kai

AN Hui-wei

XIE Zhu-tian

HE Min-xia

ZHANG Jing

WANG Chun-hua

WANG Yong

Related Institution

Zhejiang Chinese Medical University

School of Pharmacy,Shenyang Pharmaceutical University

Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences

Institute of Material Medica,Key Laboratory of Advanced Drug Delivery of Guangdong Province,Guangdong Pharmaceutical College

Foshan Fengliaoxing Pharmaceutical Co.,Ltd

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