Determination of Arctiin in Jingju Ganmao Tablets by HPLC

LIAO Xiao-ming1; ZHENG Dan2; SONG Zhi-juan2; MA Ren-qiang2

doi:10.13422/j.cnki.syfjx.2012.04.039

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Determination of Arctiin in Jingju Ganmao Tablets by HPLC

更新时间：2024-09-23

- Determination of Arctiin in Jingju Ganmao Tablets by HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 4, Pages: 113-115(2012)
- 作者机构：
  
  1. 深圳市康哲药业有限公司
  2. 广州博济医药生物技术有限公司
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2012.04.039
  CLC： R286.0
- Published：2012
- 稿件说明：
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[1]廖晓鸣,郑丹,宋志娟,马仁强.HPLC测定荆菊感冒片中牛蒡苷的含量[J].中国实验方剂学杂志,2012,18(04):113-115.

LIAO Xiao-ming1, ZHENG Dan2, SONG Zhi-juan2, et al. Determination of Arctiin in Jingju Ganmao Tablets by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(4): 113-115.
[1]廖晓鸣,郑丹,宋志娟,马仁强.HPLC测定荆菊感冒片中牛蒡苷的含量[J].中国实验方剂学杂志,2012,18(04):113-115. DOI： 10.13422/j.cnki.syfjx.2012.04.039.

LIAO Xiao-ming1, ZHENG Dan2, SONG Zhi-juan2, et al. Determination of Arctiin in Jingju Ganmao Tablets by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(4): 113-115. DOI： 10.13422/j.cnki.syfjx.2012.04.039.

摘要

目的:建立荆菊感冒片中牛蒡苷的含量测定方法。方法:采用高效液相色谱法

以VARIAN Microsorb 100-5 C18柱为分析柱

甲醇-水（40∶60）为流动相

流速1.0 mL.min-1

检测波长为280 nm。结果:牛蒡苷在0.042 8～0.856 g.L-1线性关系良好

r=0.999 9;平均加样回收率为100.2%

RSD 1.45%（n=6）。结论:该方法简便、快速、准确

可用于测定荆菊感冒片中牛蒡苷的含量。

Abstract

Objective:To establish a HPLC method to determine arctiin in Jingju Ganmao tablets.Method:The determination was conducted by HPLC using a VARIAN Microsorb 100-5 C18 column.The mobile phase consisted of CH3OH∶ H2O（40∶ 60） with flow rate of 1.0 mL.min-1 and the detection wavelength was 280 nm.Result:This method had good resolution and good linear relationship between 0.042 8-0.856 g.L-1.The averagere covery of arctiin was 100.2% and RSD was 1.45%（n=6）.Conclusion:This method is simple

quick and accurate.It can be used for quantity control of Jingju Ganmao tablets.

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Related Author

LIAO Xiao-ming

ZHENG Dan

SONG Zhi-juan

MA Ren-qiang

WANG Zhao-hua

ZHANG Da-jun

ZHAO Yu-lan

XU Guo-jing

Related Institution

Jilin Agricultural University

Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences

Chengde Medical University

Jilin Huakang Pharmaceutical Co. Ltd.

The First Clinical Medical College of Guangzhou University of Chinese Medicine

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