Fingerprint Research of Semen Armeniacae Semen Amarum

WEI Hui-zhen1; WANG Xin2; WANG Yue-sheng1; RAO Yi1; HU Jing-ting2

doi:10.13422/j.cnki.syfjx.2012.08.037

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Fingerprint Research of Semen Armeniacae Semen Amarum

更新时间：2024-09-23

- Fingerprint Research of Semen Armeniacae Semen Amarum
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 8, Pages: 71-74(2012)
- 作者机构：
  
  1. 中药固体制剂制造技术国家工程研究中心
  2. 江西中医学院
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2012.08.037
  CLC： R284.1
- Published：2012
- 稿件说明：
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[1]魏惠珍,王信,王跃生,饶毅,胡景婷.炒苦杏仁饮片指纹图谱研究[J].中国实验方剂学杂志,2012,18(08):71-74.

WEI Hui-zhen1, WANG Xin2, WANG Yue-sheng1, et al. Fingerprint Research of Semen Armeniacae Semen Amarum[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(8): 71-74.
[1]魏惠珍,王信,王跃生,饶毅,胡景婷.炒苦杏仁饮片指纹图谱研究[J].中国实验方剂学杂志,2012,18(08):71-74. DOI： 10.13422/j.cnki.syfjx.2012.08.037.

WEI Hui-zhen1, WANG Xin2, WANG Yue-sheng1, et al. Fingerprint Research of Semen Armeniacae Semen Amarum[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(8): 71-74. DOI： 10.13422/j.cnki.syfjx.2012.08.037.

摘要

目的:建立炒苦杏仁饮片的高效液相指纹图谱

提高药材质量控制水平。方法:采用高效液相色谱法

C18色谱柱

流动相乙腈-0.1%磷酸

流速1 mL·min-1

检测波长225 nm。采用国家食品药品监督管理局推荐的"中药色谱指纹图谱相似度评价系统（2004A版）"计算处理

确定了炒苦杏仁饮片指纹图谱研究方法。结果:各批次药材共获得10个共有峰

超过总面积95%

所得指纹图谱方法学考察结果良好

采用色谱指纹图谱相似度评价软件

对炒苦杏仁饮片指纹图谱进行相似度计算

其10批样品相似度在0.5～0.9。结论:指纹图谱的运用实现了炒苦杏仁饮片的全面和整体评价

能体现炒苦杏仁饮片的多个成分的指纹信息

为有效提高炒苦杏仁饮片质量控制提供参考。

Abstract

Objective:To instruct the fingerprint of Armeniacae Semen Amarum

enhance the method of quality control.Method: The separation was performed on an C18 chromatography column

using acetonitrile-0.1% of phosphoric acid as mobile phase

with the flow rate of 1 mL·min-1;the wavelength was set at 225 nm.’TCM chromatographic fingerprint similarity evaluation system（2004A edition）’ recommended by state food and drug administration was used for calculating

to determine the methods of Armeniacae Semen Amarum fingerprint research.Result: Methodology of fingerprint investigation results is qualified;the similarity in 10 batch samples was between 0.5 and 0.9.Conclusion: The characteristics of large difference absorption wavelength of multiple components for effectively improve fingerprint information

Armeniacae Semen Amarum decoction pieces quality control to provide the reference.

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Related Author

WEI Hui-zhen

WANG Xin

WANG Yue-sheng

RAO Yi

HU Jing-ting

Zi-jing XUE

Dan ZHANG

Long GUO

Related Institution

Traditional Chinese Medicine Processing Technology Innovation Center of Hebei Province， College of Pharmacy，Hebei University of Chinese Medicine

Hebei College of Chemical and Pharmaceutical Technology

National Resource Center for Chinese Materia Medica，China Academy of Chinese Medical Sciences

Center for Drug Evaluation，National Medical Products Administration

School of Pharmacy，Shandong University of Traditional Chinese Medicine

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