Stability of Chemical Reference Rubrofusarin-6-O-β-gentiobioside of Semen Cassiae

JIANG Yan-yan; XU Dong-yan; WANG Yue-ming; LIU Hui; LIU Bin; SHI Ren-bing

doi:10.13422/j.cnki.syfjx.2012.09.025

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Stability of Chemical Reference Rubrofusarin-6-O-β-gentiobioside of Semen Cassiae

更新时间：2024-09-23

- Stability of Chemical Reference Rubrofusarin-6-O-β-gentiobioside of Semen Cassiae
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 9, Pages: 142-145(2012)
- 作者机构：
  
  北京中医药大学中药学院
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2012.09.025
  CLC： R284.1
- Published：2012
- 稿件说明：
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[1]姜艳艳,徐冬艳,王月明,刘慧,刘斌,石任兵.决明子中化学对照品红镰霉素龙胆二糖苷稳定性[J].中国实验方剂学杂志,2012,18(09):142-145.

JIANG Yan-yan, XU Dong-yan, WANG Yue-ming, et al. Stability of Chemical Reference Rubrofusarin-6-O-β-gentiobioside of Semen Cassiae[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(9): 142-145.
[1]姜艳艳,徐冬艳,王月明,刘慧,刘斌,石任兵.决明子中化学对照品红镰霉素龙胆二糖苷稳定性[J].中国实验方剂学杂志,2012,18(09):142-145. DOI： 10.13422/j.cnki.syfjx.2012.09.025.

JIANG Yan-yan, XU Dong-yan, WANG Yue-ming, et al. Stability of Chemical Reference Rubrofusarin-6-O-β-gentiobioside of Semen Cassiae[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(9): 142-145. DOI： 10.13422/j.cnki.syfjx.2012.09.025.

摘要

目的:研究决明子中化学对照品红镰霉素龙胆二糖苷的稳定性。方法:将红镰霉素-6-O-β-龙胆二糖苷分别置于不同温度、湿度及不同溶剂环境下处理

采用高效液相色谱法测定含量

计算剩余率。结果:温度对红镰霉素龙胆二糖苷的稳定性影响较大

湿度影响次之

温度、湿度越高

稳定性越差;红镰霉素龙胆二糖苷在甲醇、乙醇中较为稳定

在水、0.1%盐酸溶液稳定性次之

在0.1%氨水溶液中稳定性最差。结论:红镰霉素龙胆二糖苷应置于干燥器中低温或室温密封保存;红镰霉素龙胆二糖苷对照品溶液应选择甲醇和乙醇为溶剂

低温保存。

Abstract

Objective: To study the stability of rubrofusarin-6-O-β-gentiobioside of Semen Cassiae.Method: Rubrofusarin-6-O-β-gentiobioside was processed under different temperature

humidity and solvent respectively.The content was determined by HPLC and the remaining percentages of rubrofusarin-6-O-β-gentiobioside were calculated.Result: The stability of rubrofusarin-6-O-β-gentiobioside was influenced mostly by temperature

and secondly by humidity.The stability of rubrofusarin-6-O-β-gentiobioside reduced along with the temperature rising and the humidity increasing;rubrofusarin-6-O-β-gentiobioside was much more stable in methanol and ethanol than in water and 0.1% hydrochloric acid aqueous solution

and rubrofusarin-6-O-β-gentiobioside transferred to other substance in 0.1% ammonia aqueous solution.Conclusion: Rubrofusarin-6-O-β-gentiobioside should be preserved under low or room temperature in dry condition.Methanol or ethanol should be selected as solvent of rubrofusarin-6-O-β-gentiobioside solution

preserved under low temperature.

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Related Author

JIANG Yan-yan

XU Dong-yan

WANG Yue-ming

LIU Hui

LIU Bin

SHI Ren-bing

ZHANG Sheng-tan

WANG Tie-shan

Related Institution

Department of Pharmacy,Zhujiang Hospital,Southern Medical University

Hospital of Chengdu University of Traditional Chinese Medicine （TCM）

School of TCM，Capital Medical University

School of Pharmacy，Nanjing University of Chinese Medicine

Jiangsu Institute for Food and Drug Control

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