Simultaneous Determination of Calycosin Glycoside、 Atractylenolide-1,Atractylenolide Ⅲ in Crude Extract of Radix Astragali-Atractylodis Macrocephalae Herb Couple by HPLC
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Simultaneous Determination of Calycosin Glycoside、 Atractylenolide-1,Atractylenolide Ⅲ in Crude Extract of Radix Astragali-Atractylodis Macrocephalae Herb Couple by HPLC
Chinese Journal of Experimental Traditional Medical FormulaeVol. 18, Issue 9, Pages: 86-89(2012)
ZHANG Ying-feng1, ZHU Li-xia2, LIANG Dong-hui2, et al. Simultaneous Determination of Calycosin Glycoside、 Atractylenolide-1,Atractylenolide Ⅲ in Crude Extract of Radix Astragali-Atractylodis Macrocephalae Herb Couple by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(9): 86-89.
ZHANG Ying-feng1, ZHU Li-xia2, LIANG Dong-hui2, et al. Simultaneous Determination of Calycosin Glycoside、 Atractylenolide-1,Atractylenolide Ⅲ in Crude Extract of Radix Astragali-Atractylodis Macrocephalae Herb Couple by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(9): 86-89. DOI: 10.13422/j.cnki.syfjx.2012.09.073.
Simultaneous Determination of Calycosin Glycoside、 Atractylenolide-1,Atractylenolide Ⅲ in Crude Extract of Radix Astragali-Atractylodis Macrocephalae Herb Couple by HPLC
Objective: To establish a new RP-HPLC method for simultaneous determination of calycosin
atractylenolide-1
atractylenolide Ⅲ in crude extract of Radix astragali-Atractylodis Macrocephalae herb couple.Method: Analysis was carried out on a Kromasil 100-5C18(4.6 mm×250 mm) column with acetonitrile-pure water as mobile phases in gradient elution.The flow rate was 1 mL·min-1
and the UV detector was monitored at 220 nm.Result:All calibration curve showed good linear regression in test ranges(r>0.999 5);and the overall recoveries were in the range of 97%-103%(n=3)with RSD less than 3%.The overall RSD of precision test was less than 3%.Conclusion: The method is rapid
acute
credible and repeatable
and can provide bases for the material basis and compatibility for Radix astragali-Atractylodis Macrocephalae herb couple.
Simultaneous Determination of Calycosin Glycoside、 Atractylenolide-1, Atractylenolide Ⅲ in Crude Extract of Radix Astragali- Atractylodis Macrocephalae Herb Couple by HPLC
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Related Author
ZHANG Ying-feng
ZHU Li-xia
LIANG Dong-hui
WU Yang
ZHANG Ke-wei
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