Microwave Extraction and Spectral Analysis of the Total Polysaccharides in Sijunzi Decoction

WANG Ying-li; WANG Xiu-wen; ZENG Dong-ming; LIU Ya-ming

doi:10.13422/j.cnki.syfjx.2012.16.073

您当前的位置：

首页 >

文章列表页 >

Microwave Extraction and Spectral Analysis of the Total Polysaccharides in Sijunzi Decoction

更新时间：2024-09-23

- Microwave Extraction and Spectral Analysis of the Total Polysaccharides in Sijunzi Decoction
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 16, Pages: 77-80(2012)
- 作者机构：
  
  山西中医学院中药系
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2012.16.073
  CLC： R284.1
- Published：2012
- 稿件说明：
移动端阅览
[1]王颖莉,王秀文,曾冬明,刘亚明.四君子汤(党参)多糖的微波法提取工艺及其光谱分析[J].中国实验方剂学杂志,2012,18(16):77-80.

WANG Ying-li, WANG Xiu-wen, ZENG Dong-ming, et al. Microwave Extraction and Spectral Analysis of the Total Polysaccharides in Sijunzi Decoction[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(16): 77-80.
[1]王颖莉,王秀文,曾冬明,刘亚明.四君子汤(党参)多糖的微波法提取工艺及其光谱分析[J].中国实验方剂学杂志,2012,18(16):77-80. DOI： 10.13422/j.cnki.syfjx.2012.16.073.

WANG Ying-li, WANG Xiu-wen, ZENG Dong-ming, et al. Microwave Extraction and Spectral Analysis of the Total Polysaccharides in Sijunzi Decoction[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(16): 77-80. DOI： 10.13422/j.cnki.syfjx.2012.16.073.

摘要

目的:优选四君子汤总多糖的微波提取适宜条件。方法:利用微波法进行工艺条件的改进

通过正交试验设计对总多糖提取参数进行了优选

对提取的总多糖采用红外吸收光谱和紫外吸收光谱进行分析表征。结果:微波法适合于提取四君子汤的总多糖

是一种优于传统水煎煮法、提取效率高、用时少的新的提取法。适宜的提取工艺条件是390 W的功率下

以1∶20的液固比提取6 min

提取2次

此条件下多糖含量为14.82%

比实验条件下的传统法提高了10.26%。红外光谱分析显示微波法提取的多糖的结构与传统法基本一致

且证明多糖主要来源于党参的提取物。结论:微波法提取时间短、效率高

适合于提取四君子汤的总多糖。

Abstract

Objective:To select the optimum microwave extracting conditions for polysaccharide.Method: Based on the design of the orthogonal experimental

the optimum extracting conditions for polysaccharide were optimized.The content of polysaccharide was detected by phenol-sulfuric acid

and the structure of polysaccharide was analyzed by infrared spectrum.Result: The results show that the optimum microwave extraction conditions are 390 W power

1∶20 liquid material ratio

6 min for 2 times.Under these operating conditions

the polysaccharide content is 14.82%

which is obviously higher than 10.26% obtained by the traditional method.Infrared analysis showed that the structure of polysaccharide from microwave extraction is basically the same as the traditional method.The microwave method is reasonable for the extraction total polysaccharide in the Sijunzi decoctin and it has the advantages of the high efficiency and save time.Conclusion: The microwave extraction can save time

and has higher efficiency than the traditional method.It was reasonable for total polysaccharides of Sijunzi decoctin.

关键词

Keywords

references

Views

332

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Complex Purification Technology of Effective Parts from Astragali Radix

Optimization of Extraction Technology for Polysaccharide from Sugarcane Leaves by Orthogonal Test with Multi-index

Optimization of Vacuum Reflux Extraction Technology for Total Flavonoids from

Optimization of Extraction Process of Total Polysaccharides in Bupleuri Radix and Its Content Difference in Different Processed Products of Bupleuri Radix

Related Author

WANG Ying-li

WANG Xiu-wen

ZENG Dong-ming

LIU Ya-ming

DUAN Li-jun

SUN Bo-hang

WU Yu-qiang

HOU Xiao-tao

Related Institution

Beijing University of Chinese Medicine

Beijing Key Laboratory of Chinese Materia Pharmacology，Institute of Basic Medical Sciences， Xiyuan Hospital，China Academy of Chinese Medical Sciences

Natural History Museum of China

Institute of Chinese Materia Medica，China Academy of Chinese Medical Sciences

Jiangxi University of Chinese Medicine

AI问答

Postal code：100700
Tel：010-84076882 Email：syfjx_2010@188.com
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备11006657号-10 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰