Content Determination of Salvianolic Acid B in Yishen Juanbi Capsule by HPLC

LI Jun-fang; CUI Ya-hui; ZHENG Yan-chun; DONG Hai-rong; HUANG Fei-long

doi:10.13422/j.cnki.syfjx.2012.18.003

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Content Determination of Salvianolic Acid B in Yishen Juanbi Capsule by HPLC

更新时间：2024-09-23

- Content Determination of Salvianolic Acid B in Yishen Juanbi Capsule by HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 18, Issue 18, Pages: 103-105(2012)
- 作者机构：
  
  承德颈复康药业集团有限公司河北省中药新辅料工程技术研究中心
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2012.18.003
  CLC： O657.72;R286.0
- Published：2012
- 稿件说明：
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[1]李俊芳,崔雅慧,郑艳春,董海荣,黄飞龙.HPLC测定蚁参蠲痹胶囊中丹酚酸B的含量[J].中国实验方剂学杂志,2012,18(18):103-105.

LI Jun-fang, CUI Ya-hui, ZHENG Yan-chun, et al. Content Determination of Salvianolic Acid B in Yishen Juanbi Capsule by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(18): 103-105.
[1]李俊芳,崔雅慧,郑艳春,董海荣,黄飞龙.HPLC测定蚁参蠲痹胶囊中丹酚酸B的含量[J].中国实验方剂学杂志,2012,18(18):103-105. DOI： 10.13422/j.cnki.syfjx.2012.18.003.

LI Jun-fang, CUI Ya-hui, ZHENG Yan-chun, et al. Content Determination of Salvianolic Acid B in Yishen Juanbi Capsule by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(18): 103-105. DOI： 10.13422/j.cnki.syfjx.2012.18.003.

摘要

目的:建立蚁参蠲痹胶囊中丹酚酸B的含量测定方法。方法:采用高效液相色谱法测定蚁参蠲痹胶囊中丹酚酸B的含量。色谱法分析条件为Kromasil-C18柱（4.6 mm×250 mm

5μm）

流动相甲醇-乙腈-1.7%甲酸水溶液（28∶8∶64）

流速1.0 mL.min-1

检测波长286 nm。结果:丹酚酸B在0.150 4～15.04μg与峰面积呈良好的线性关系（r=0.999 9）

平均回收率98.90%

RSD 1.22%。结论:该方法操作简便

结果可靠

为蚁参蠲痹胶囊的质量研究提供有效的方法。

Abstract

Objective:To establish a method for determing Salvianolic acid B in Yishen Juanbi capsule.Method: Determination of salvianolic acid B in Yishen Juanbi capsule was performed on Kromasil-C18 column（4.6 mm×250 mm

5 μm）;mobile phase was methanol-acetonitrile-1.7% formic acid solution（28∶8∶64）;flow rate was 1.0 mL · min-1;detection wavelength was set at 286 nm.Result:Salvianolic acid B was linear in the range of 0.150 4-15.04 μg（r=0.999 9）;the average recovery was 98.90%

RSD 1.22%.Conclusion:This method has good repeatability and flexibility.It can be used for quality control in production of Yishen Juanbi capsule.

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Related Author

LI Jun-fang

CUI Ya-hui

ZHENG Yan-chun

DONG Hai-rong

HUANG Fei-long

ZHANG Ke-wei

WU Hao

CUI Xiao-bing

Related Institution

Jiangxi College of Traditional Chinese Medicine

Dali University,Dali

Level 3 Laboratory for State Administration of Traditional Chinese Medicine,Beijing Zhendong Guangming Pharmaceutical Research Institute Co.,Ltd

Institute of Chinese Meteria Medica,China Academy of Chinese Medical Sciences

Guangzhou University of Traditional Chinese Medicine

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