Investigation of Extraction and Separation Technology for Aboveground Part of Cimicifuga dahurica

SU Zhan-hui1; ZHANG Zi-ming2; WANG Shu-jun3; QIU Dong-shuang1; LIU Zhi-chao1; SUN Ya-ke1; ZHANG Yi-nan1

doi:10.13422/j.cnki.syfjx.2013.05.033

您当前的位置：

首页 >

文章列表页 >

Investigation of Extraction and Separation Technology for Aboveground Part of Cimicifuga dahurica

更新时间：2024-09-23

- Investigation of Extraction and Separation Technology for Aboveground Part of Cimicifuga dahurica
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 5, Pages: 10-13(2013)
- 作者机构：
  
  1. 承德医学院中药研究所河北省中药研究与开发重点实验室
  2. 承德市妇幼保健院
  3. 承德医学院附属医院
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2013.05.033
  CLC： R284
- Published：2013
- 稿件说明：
移动端阅览
[1]苏占辉,张滋明,王书君,邱东爽,刘志超,孙亚克,张依楠.兴安升麻地上部分的提取分离工艺考察[J].中国实验方剂学杂志,2013,19(05):10-13.

SU Zhan-hui1, ZHANG Zi-ming2, WANG Shu-jun3, et al. Investigation of Extraction and Separation Technology for Aboveground Part of Cimicifuga dahurica[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(5): 10-13.
[1]苏占辉,张滋明,王书君,邱东爽,刘志超,孙亚克,张依楠.兴安升麻地上部分的提取分离工艺考察[J].中国实验方剂学杂志,2013,19(05):10-13. DOI： 10.13422/j.cnki.syfjx.2013.05.033.

SU Zhan-hui1, ZHANG Zi-ming2, WANG Shu-jun3, et al. Investigation of Extraction and Separation Technology for Aboveground Part of Cimicifuga dahurica[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(5): 10-13. DOI： 10.13422/j.cnki.syfjx.2013.05.033.

摘要

目的:优选兴安升麻地上部分总皂苷的提取分离工艺。方法:以总皂苷含量为指标

采用分段萃取法用不同试剂萃取升麻地上部分中的有效成分

旋转蒸发回收溶剂

将正丁醇萃取物通过大孔吸附树脂柱进一步分离

并通过紫外分光光度计进行定量检测。结果:采用正丁醇萃取后得到的物质过大孔吸附树脂后

总皂苷纯度>50%。结论:通过萃取将升麻地上部分进一步分离

把有效成分按极性分段

便于后期对兴安升麻地上部分总皂苷进一步分离纯化

同时能得到较高纯度的总皂苷。

Abstract

Objective:To optimize extraction and separation technology of total saponins from aboveground part of Cimicifuga dahurica.Method:With the content of total saponins as index

segmented extraction method was used to extract active ingredients from aboveground part of C.dahurica with different reagents

solvent was recovered by rotary evaporation

then n-butanol extract was further separated by macroporous resin column

and quantitative detection was determined by UV spectrophotometer.Result:After n-butanol extraction substances over macroporous adsorption resin

purity of total saponins could reach more than 50%.Conclusion:After aboveground part of C.dahurica was further separated by extracting

active ingredients were segmented according to polarity

it could facilitate for late further separation and purification of total saponins from aboveground part of C.dahurica

at the same time

high purity of total saponins could obtain.

关键词

Keywords

references

Views

180

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Investigation of Extraction and Separation Technology for Aboveground Part of

Optimization of Extraction and Purification Process of Total Iridoids and Total Crocins in Gardeniae Fructus

Investigation of Adsorption and Desorption Properties of Total Ginsenosides on Anion-exchange Resins and Its LC-MS Analysis

LCMS-IT-TOF Analysis of Retention Behavior of Sanguisorbae Radix Components on D101 Macroporous Resin and Polyamide Resin

Optimization of Purification Process of Total Alkaloid Extract of Berberis dictyophylla Cortex by Macroporous Resin and Investigation of Its Quality Standard

Related Author

SU Zhan-hui

ZHANG Zi-ming

WANG Shu-jun

QIU Dong-shuang

LIU Zhi-chao

SUN Ya-ke

ZHANG Yi-nan

Bing-bing ZHANG

Related Institution

Institute of Chinese Materia Medica，China Academy of Chinese Medical Sciences

School of Pharmacy， Jiangxi University of Chinese Medicine

School of Pharmacy，Tianjin University of Traditional Chinese Medicine

Changchun University of Chinese Medicine

Development Center of Modern Chinese Medicine,Research Institute of Tasly Holding Group Co.Ltd.

AI问答

Postal code：100700
Tel：010-84076882 Email：syfjx_2010@188.com
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备11006657号-10 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰