Determination of Paeoniflorin in Pishen Liangzhu Pills by HPLC

DENG Shuang-bing1; SHI Yan2; HU Yu-hua1; LI Jun-hong1; LI Yan-yu1; HAI Li-na1; QIN Wen-jie1

doi:10.13422/j.cnki.syfjx.2013.05.058

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Determination of Paeoniflorin in Pishen Liangzhu Pills by HPLC

更新时间：2024-09-23

- Determination of Paeoniflorin in Pishen Liangzhu Pills by HPLC
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 19, Issue 5, Pages: 123-125(2013)
- 作者机构：
  
  1. 北京振东光明药物研究院有限公司国家中医药三级实验室
  2. 中国食品药品检定研究院
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2013.05.058
  CLC： R286.0
- Published：2013
- 稿件说明：
移动端阅览
[1]邓双炳,石岩,胡玉花,李军红,李炎玉,海丽娜,秦文杰.HPLC测定脾肾两助丸中芍药苷的含量[J].中国实验方剂学杂志,2013,19(05):123-125.

DENG Shuang-bing1, SHI Yan2, HU Yu-hua1, et al. Determination of Paeoniflorin in Pishen Liangzhu Pills by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(5): 123-125.
[1]邓双炳,石岩,胡玉花,李军红,李炎玉,海丽娜,秦文杰.HPLC测定脾肾两助丸中芍药苷的含量[J].中国实验方剂学杂志,2013,19(05):123-125. DOI： 10.13422/j.cnki.syfjx.2013.05.058.

DENG Shuang-bing1, SHI Yan2, HU Yu-hua1, et al. Determination of Paeoniflorin in Pishen Liangzhu Pills by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(5): 123-125. DOI： 10.13422/j.cnki.syfjx.2013.05.058.

摘要

目的:提高脾肾两助丸的质量标准

建立脾肾两助丸中芍药苷的含量测定方法。方法:采用高效液相色谱法

以乙腈-0.05 mol.L-1磷酸二氢钾（10∶90）为流动相

色谱柱为Kromasil-C18（4.6 mm×250 mm

5μm）

检测波长230 nm。结果:芍药苷进样量在0.106 2～1.062μg与峰面积线性关系良好（r=0.999 95）

平均回收率为96.83%。结论:方法专属性强

准确、简便

可用于脾肾两助丸的质量控制。

Abstract

Objective:To improve the quality standard of Pishen Liangzhu pills

the study of HPLC methodology was carried out to determine the paeoniflorin in the pills.Method: Using HPLC.The separation was performed on Kromasil-C18 column（4.6 mm×250 mm

5 μm）

using a mixture of acetonitrile-0.05 mol·L-1 potassium dihydrogen phosphate（10∶ 90） as the mobile phase;the detection wavelength was wet at 230 nm.Result: The calibration curve was linear within the range of 0.106 2-1.062 μg（r=0.999 95）.The average recovery for paeoniflorin was 96.83%.Conclusion: The method is selective

accurate and simple.It is suitable for controlling the quality of Pishen Liangzhu pills.

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Related Author

DENG Shuang-bing

SHI Yan

HU Yu-hua

LI Jun-hong

LI Yan-yu

HAI Li-na

QIN Wen-jie

MENG Xian-bo

Related Institution

The First Clinical Medical College of Guangzhou University of Chinese Medicine

School of Pharmaceutical Sciences, Guangzhou University of Chinese Medicine

National Resource Center for Chinese Materia Medica, China Academy of Chinese Medical Sciences

The First Affiliated Hospital of Guangzhou University of Chinese Medicine

Shanxi University of Traditional Chinese Medicine

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