Optimization of Processing Technology of  Stir-baked with Vinegar by Orthogonal Test

DENG Xu-kun; JIANG Jie; LIN Qin-xiong; CHEN Lv-yi; CAI Shuang; WU Fei; GAO Kang-li; ZHANG Di; ZHANG Jin

doi:10.13422/j.cnki.syfjx.2014100023

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Optimization of Processing Technology of Stir-baked with Vinegar by Orthogonal Test

更新时间：2024-01-04

- Optimization of Processing Technology of Stir-baked with Vinegar by Orthogonal Test
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 20, Issue 10, Pages: 23-25(2014)
- 作者机构：
- 作者简介：
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- DOI：10.13422/j.cnki.syfjx.2014100023
  CLC： R29
- Published：2014
- 稿件说明：
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DENG Xu-kun, JIANG Jie, LIN Qin-xiong, et al. Optimization of Processing Technology of Stir-baked with Vinegar by Orthogonal Test[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(10): 23-25.
DOI：

DENG Xu-kun, JIANG Jie, LIN Qin-xiong, et al. Optimization of Processing Technology of Stir-baked with Vinegar by Orthogonal Test[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(10): 23-25. DOI： 10.13422/j.cnki.syfjx.2014100023.

摘要

目的：优选江边一碗水的醋炙工艺。方法：以鬼臼毒素含量为指标，通过正交试验考察闷润时间、醋用量、炒制时间、炒制温度对醋炙工艺的影响。采用HPLC测定鬼臼毒素含量，流动相甲醇-0.1 moL·L-1磷酸二氢钾水溶液（45∶55），检测波长290 nm。结果：最佳炮制工艺为醋用量30%，闷润时间2 h，炒制温度150 ℃，炒制时间4 min；醋用量、炒制时间对醋炙工艺的影响具有显著性意义，鬼臼毒素质量分数达5.48%。结论：该炮制工艺合理可行，可为江边一碗水的民间安全用药提供参考。

Abstract

Objective: To optimize processing technology of Diphylleia sinensis stir-baked with vinegar. Method: Taking the content of podophyllotoxin as index

orthogonal test was adopted to optimize processing technology with four factors including moistening time

the amount of vinegar

frying time and temperature.With mobile phase of methanol-0.1 mol·L-1 potassium dihydrogen phosphate solution(45∶55) and detection wavelength at 290 nm

the content of podophyllotoxin was determined by HPLC. Result: The best processing technology was as following:moistened 2 h with 30% vinegar

flew 4 min at 150 ℃.The amount of vinegar and frying time had significantly effects on processing technology

the mass fraction of podophyllotoxin was up to 5.48%. Conclusion: This optimized processing technology was reasonable and feasible.This result could provide a reference for medication safety of D. sinensis in folk.

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Related Institution

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