Optimization of Extraction Process for Volatile Oil from by Central Composite Design-response Surface Methodology

WANG Bai-ling; WANG Shu-mei; MENG Jiang; WANG Guo-cai; LIANG Sheng-wang

doi:10.13422/j.cnki.syfjx.2014110037

您当前的位置：

首页 >

文章列表页 >

Optimization of Extraction Process for Volatile Oil from by Central Composite Design-response Surface Methodology

更新时间：2024-01-04

- Optimization of Extraction Process for Volatile Oil from by Central Composite Design-response Surface Methodology
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 20, Issue 11, Pages: 37-40(2014)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2014110037
  CLC： TQ461;R284.2
- Published：2014
- 稿件说明：
移动端阅览
WANG Bai-ling, WANG Shu-mei, MENG Jiang, et al. Optimization of Extraction Process for Volatile Oil from by Central Composite Design-response Surface Methodology[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(11): 37-40.
DOI：

WANG Bai-ling, WANG Shu-mei, MENG Jiang, et al. Optimization of Extraction Process for Volatile Oil from by Central Composite Design-response Surface Methodology[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(11): 37-40. DOI： 10.13422/j.cnki.syfjx.2014110037.

摘要

目的：优选鸡骨香挥发油的提取工艺条件。方法：采用水蒸气蒸馏法提取鸡骨香中挥发油，选取挥发油得率和cypenrenoic acid提取量的总评“归一值”为因变量，采用星点设计考察液料比、浸泡时间和提取时间对提取工艺的影响，对试验数据进行多元线性回归和二项式拟合，运用效应面法优选提取工艺并进行预测分析。结果：评价指标的二项式拟合方程（r=0.993）优于多元线性回归方程（r=0.804），最佳提取工艺为加17.57倍量水浸泡101.75 min，提取时间321.29 min；挥发油平均得率4.06%，cypenrenoic acid提取量0.143 mg·g-1，与预测值的偏差分别为1.44%，2.569%。结论：该优选工艺简便、预测性良好，为鸡骨香的资源开发提供参考。

Abstract

Objective:To optimize extraction process of volatile oil from Croton crassifolius. Method:Volatile oil from C. crassifolius was extracted by steam distillation method

with "overall desirability" of yield of volatile oil and the concentration of cypenrenoic acid as dependent variable

the amount of water

soaking time and extracting time were investigated by central composite design

test data were fitted by multi-linear equation and second-order polynomial equation

extraction technology conditions were optimized by response surface methodology and to predictive analysis. Result:Multiple correlation coefficients from second-order polynomial equation(r=0.993) were prior to those from multi-linear equation(r=0.804)

optimum extraction process conditions were as follows:soaked 101.75 min with 17.57 times the amount of water

distillation time of 321.29 min;under these conditions

average yield of volatile oil was 4.06%

extracting amount of cypenrenoic acid was 0.143 mg·g-1

deviations between observed and predicted values were less than 3%. Conclusion:This optimized process was simple with high predictability

it could provide test basis for resource development of C. crassifolius.

关键词

Keywords

references

Views

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Optimization of Extraction Process of Volatile Oil from Guanxinkang Capsule by Central Composite Design-Response Surface Methodology

Optimum Extraction Technology for Volatile Oil from Seeds of

Optimization of Extraction Technology for by Central Composite Design-Response Surface Methodology

Optimization of Extraction Technology for Volatile Oil from Roots of in Guizhou Province and GC-MS Analysis of Its Chemical Composition

Optimization of Preparation Technology of -Cyclodextrin Inclusion Complexes for Volatile Oil in Guanxinkang Capsule

Related Author

SHI Ming-yi

LI Jian-li

XIE Yan

YANG Shan

XI Jian

WANG Li-jie

HE Hua

LI Xian-kuan

Related Institution

State Key Laboratory of Southwestern Chinese Medicine Resources， Chengdu University of Traditional Chinese Medicine

College of Pharmacy， Heilongjiang University of Chinese Medicine

Basic Medical College， Heilongjiang University of Chinese Medicine

Hubei Research Center of Chinese Materia Medica Processing Engineering and Technology， School of Pharmacy，Hubei University of Chinese Medicine

National Engineering Laboratory for Quality Control Technology of Chinese Materia Medica， Institute of Chinese Materia Medica，China Academy of Chinese Medical Sciences

AI问答

Postal code：100700
Tel：010-84076882 Email：syfjx_2010@188.com
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备11006657号-10 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰