Quality Standard for Tongfenglixiao Preparations

GAO Ya-feng; SUN Da-zhong; WANG Jun-song; ZHANG Xiao-dong; WANG Pei

doi:10.13422/j.cnki.syfjx.2014130069

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Quality Standard for Tongfenglixiao Preparations

更新时间：2024-01-04

- Quality Standard for Tongfenglixiao Preparations
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 20, Issue 13, Pages: 69-72(2014)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2014130069
  CLC： R286.0
- Published：2014
- 稿件说明：
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GAO Ya-feng, SUN Da-zhong, WANG Jun-song, et al. Quality Standard for Tongfenglixiao Preparations[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(13): 69-72.
DOI：

GAO Ya-feng, SUN Da-zhong, WANG Jun-song, et al. Quality Standard for Tongfenglixiao Preparations[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(13): 69-72. DOI： 10.13422/j.cnki.syfjx.2014130069.

摘要

目的：建立痛风立消制剂的质量标准。方法：采用薄层色谱法对土茯苓、木瓜、石菖蒲、乌药、萆薢等进行定性鉴别；采用紫外分光光度法对制剂中柚皮苷进行含量测定；采用高效液相色谱法对制剂中绿原酸进行含量测定。结果：柚皮苷在0.056~0.196 mg（r=0.999 9）与吸收度呈良好的线性关系，平均回收率99.31%，RSD 0.56%；绿原酸在0.32~1.92 μg（r=0.999 7）与峰面积呈良好的线性关系。平均回收率99.66%，RSD 0.415%。结论：该方法简便易行、结果准确可靠，重复性好，可作为痛风立消制剂质量控制标准。

Abstract

Objective: To establish the quality standard of the Tongfenglixiao preparations. Method: Qualitative identification was performed by thin layer chromatography on Dioscorea collettii

Papaya

Shichangpu

Aggregata

Smilax glabra;the content was measured with UV spectrophotometry the naringin in the formulations

with HPLC method for the content of chlorogenic acid in the it. Result: The naringin and chlorogenic acid showed good linear relationship (r=0.999 9

r=0.999 7) in the range of 0.056-0.196 mg

0.32-1.92 μg. The average recovery was 99.31%

99.66% with RSD 0.56%

0.415%. Conclusion: The method is simple

accurate and reliable

reproducible and can be used as agents of Tongfenglixiao quality control standards.

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Related Institution

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