Chemical Constituents of (Ⅱ)

JIANG Xue-qing; GAN Zheng-yang; YAN Chen; LV Yang-yang; SONG Wan-ju

doi:10.13422/j.cnki.syfjx.2014160067

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Chemical Constituents of (Ⅱ)

更新时间：2024-01-04

- Chemical Constituents of (Ⅱ)
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 20, Issue 16, Pages: 67-70(2014)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2014160067
  CLC： R284.1
- Published：2014
- 稿件说明：
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JIANG Xue-qing, GAN Zheng-yang, YAN Chen, et al. Chemical Constituents of (Ⅱ)[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(16): 67-70.
DOI：

JIANG Xue-qing, GAN Zheng-yang, YAN Chen, et al. Chemical Constituents of (Ⅱ)[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(16): 67-70. DOI： 10.13422/j.cnki.syfjx.2014160067.

摘要

目的：研究黔产五香血藤的化学组成，探究其活性成分。方法：采用硅胶柱色谱、大孔树脂柱色谱、分子筛色谱、重结晶、高效液相色谱纯化等方法，从五香血藤乙醇提取物的石油醚和乙酸乙酯部分分离纯化化合物，并根据其理化性质、核磁共振氢谱、碳谱、及质谱等波谱数据鉴定结构。结果：分离并鉴定了8个化合物，分别为五内酯E甲酯（1），北五味子酸（2），sorghumol（3），黑色五味子单体苷（4），lancilactone C（5），南五味子宁（6），β-谷甾醇（7），（+）-安五脂素（8）。结论：化合物 2~5 为首次从该植物中分离得到，其中， 1，2，3，5 为三萜类化合物， 4，6，8 为木脂素类化合物。

Abstract

Objective: This study was aimed to investigate the chemical constituent of Kadsura longipeduculata collected from Guizhou province

and to explore the active ingredients in this herb. Method: Methods including silica gel column chromatography

macroporous resin column chromatography

molecular sieve chromatography

recrystallization and HPLC preparation were used. And the constituents were separated and purified from the petroleum ether and ethyl acetate fractions of ethanol extract of K. longipeduculata. According to their physical and chemical properties

coupled with the data of 1H-NMR

13C-NMR and EIS-MS

the structures were elucidated. Result: Eight compounds were isolated and identified as tubiferolide methyl ester(1)

schizandronic acid(2)

sorghumol(3)

schizandriside(4)

lancilactone C(5)

kadsurarin(6)

β-sitosterol(7)

(+)-anwulignan(8). Conclusion: Compounds 2-5 are isolated from the plant for the first time. 1

5 are triterpene compounds

and 4

8 are lignans compounds.

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