Analysis of Chemical Constituents of Volatile Oil from Domestic Folium Sennae by GC-MS

DUAN Jing-yu; WEI Xian-yong; LI Yan; YAO Huan-kai; ZHANG Chun-ping; ZONG Zhi-min

doi:10.13422/j.cnki.syfjx.2014170106

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Analysis of Chemical Constituents of Volatile Oil from Domestic Folium Sennae by GC-MS

更新时间：2024-01-04

- Analysis of Chemical Constituents of Volatile Oil from Domestic Folium Sennae by GC-MS
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 20, Issue 17, Pages: 106-109(2014)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2014170106
  CLC： O657.63;R284.1
- Published：2014
- 稿件说明：
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DUAN Jing-yu, WEI Xian-yong, LI Yan, et al. Analysis of Chemical Constituents of Volatile Oil from Domestic Folium Sennae by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(17): 106-109.
DOI：

DUAN Jing-yu, WEI Xian-yong, LI Yan, et al. Analysis of Chemical Constituents of Volatile Oil from Domestic Folium Sennae by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(17): 106-109. DOI： 10.13422/j.cnki.syfjx.2014170106.

摘要

目的：采用气相色谱-质谱联用技术（GC-MS）分析国产番泻叶中挥发油的化学成分。方法：采用水蒸气蒸馏法提取番泻叶中挥发油，通过GC-MS对挥发油的化学成分进行分析鉴定。结果：采用面积归一化法对挥发油的化学成分进行定量分析，共鉴定出21种化合物，占挥发油总量的66.996%。主要成分为法尼基丙酮（16.322%），植物醇（13.022%），角鲨烯（6.864%），6，10，14-三甲基-2-十五烷酮（6.672%），丹皮酚（5.995%）。结论：该研究结果为国产番泻叶的进一步开发利用提供了可靠的实验数据及理论依据。

Abstract

Objective: The study was performed to analyze the chemical constituents of volatile oil from domestic Folium Sennae with GC-MS technology. Method: The volatile oil was extracted from the leaves by steam distillation. The constituents of volatile oil were identified by GC-MS technology. Result: Relative content of volatile oil was determined by peak area normalization.Totally

21 compounds were identified

accounting for 66.996% of the total volatile oil content. The principal chemical constituents of the essential oils are farnesyl acetone (16.322%)

phytol (13.022%)

squalene (6.864%)

14-trimethyl-2-pentadecanone (6.672%)

paeonol (5.995%). Conclusion: The result provided reliable experimental data and theoretical bases for the further development and utilization of domestic Folium Sennae.

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Related Institution

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